Afolabi Olusegun Adigun, Mohan Turup Pandurangan, Kanny Krishnan
Composite Research Group, Department of Mechanical Engineering, Durban University of Technology, Durban 4000, South Africa.
Materials (Basel). 2023 Feb 20;16(4):1732. doi: 10.3390/ma16041732.
A solution casting approach is used to create hollow glass microsphere (HGM)-filled epoxy-syntactic foam composites (e-SFCs) by varying the concentrations of HGM in epoxy according to different particle sizes. Density analysis is used to investigate the impact of concentration and particle size regularity on the microstructure of e-SFCs. It was observed that e-SFCs filled with an HGM of uniform particle sizes exhibit a reduction in density with increasing HGM concentration, whereas e-SFCs filled with heterogeneous sizes of HGM exhibit closeness in density values regardless of HGM concentration. The variation in e-SFC density can be related to HGM packing efficiency within e-SFCs in terms of concentration and particle size regularity. The particle size with lowest true density of 0.5529 g/cm, experimental density of 0.949 g/cm and tensile strength of 55.74 MPa resulted in e-SFCs with highest specific properties of 100.81 (MPa·g/cm), with a 35.1% increase from the lowest value of 74.64 (MPa·g/cm) at a true density of 0.7286 g/cm, experimental density of 0.928 g/cm and tensile strength of 54.38 MPa. The e-SFCs' theoretical density values were obtained. The variance in theoretical and experimental density values provides a thorough grasp of packing efficiency and inter-particle features.
采用溶液浇铸法,根据不同粒径改变环氧树脂中空心玻璃微球(HGM)的浓度,以制备填充HGM的环氧复合泡沫材料(e-SFCs)。通过密度分析研究浓度和粒径规整性对e-SFCs微观结构的影响。观察到,填充粒径均匀的HGM的e-SFCs密度随HGM浓度增加而降低,而填充粒径不均一的HGM的e-SFCs,无论HGM浓度如何,密度值都较为接近。e-SFCs密度的变化在浓度和粒径规整性方面与e-SFCs内HGM的填充效率有关。真密度最低为0.5529 g/cm、实验密度为0.949 g/cm、拉伸强度为55.74 MPa的粒径,所制备的e-SFCs具有最高的比性能100.81(MPa·g/cm),相较于真密度为0.7286 g/cm、实验密度为0.928 g/cm、拉伸强度为54.38 MPa时的最低值74.64(MPa·g/cm)提高了35.1%。获得了e-SFCs的理论密度值。理论密度值与实验密度值的差异有助于深入了解填充效率和颗粒间特性。