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一种适用于长波长光驱动扫描探针显微镜的低温恒温器。

A Cryostat Applicable to Long-Wavelength Light-Driven Scanning Probe Microscopy.

作者信息

Xiang Kui, Xie Caihong, Feng Qiyuan, Wang Ze, Dai Guangbin, Wang Jihao, Zhang Jing, Meng Wenjie, Hou Yubin, Lu Qingyou, Lu Yalin

机构信息

High Magnetic Field Laboratory, Hefei Institutes of Physical Science, Chinese Academy of Sciences, Hefei 230031, China.

University of Science and Technology of China, Hefei 230026, China.

出版信息

Micromachines (Basel). 2023 Feb 2;14(2):378. doi: 10.3390/mi14020378.

DOI:10.3390/mi14020378
PMID:36838078
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC9964935/
Abstract

Recently, there has been growing interest in using lightwave-driven scanning probe microscopy (LD-SPM) to break through the Abbe diffraction limit of focusing, yielding insight into various energy couplings and conversion processes and revealing the internal information of matter. We describe a compact and efficient optical cryostat designed for LD-SPM testing under magnetic fields. The exceptional multilayer radiation shielding insert (MRSI) forms an excellent temperature gradient when filled with heat conducting gas, which removes the requirement to install an optical window in the liquid helium cooling shell. This not only critically avoids the vibration and thermal drift caused by solid heat conduction but also minimizes light transmission loss. The application of gate valves and bellows allows a simpler and more effective replacement of the sample and working cell in the test cavity. ANSYS software is used for steady-state thermal analysis of the MRSI to obtain the temperature distribution and heat transfer rate, and the necessity of the flexible copper shielding strips is illustrated by the simulations. The topography and magnetic domain images of 45 nm-thick LaCaMnO thin films on NdGaO(001) substrates under a magnetic field were obtained by a self-made lightwave-driven magnetic force microscope in this cryostat. The resolution and noise spectra during imaging reveal temperature stability and low vibration throughout the cryostat. The experience acquired during the development of this cryostat will help to establish cryostats of similar types for a variety of optic applications requiring the use of cryogenic temperatures.

摘要

最近,人们越来越关注使用光波驱动扫描探针显微镜(LD-SPM)来突破聚焦的阿贝衍射极限,深入了解各种能量耦合和转换过程,并揭示物质的内部信息。我们描述了一种紧凑高效的光学低温恒温器,专为在磁场下进行LD-SPM测试而设计。特殊的多层辐射屏蔽插入件(MRSI)在填充导热气体时形成出色的温度梯度,从而无需在液氦冷却壳中安装光学窗口。这不仅关键地避免了由固体热传导引起的振动和热漂移,还将光传输损失降至最低。闸阀和波纹管的应用使得在测试腔中更换样品和工作单元更加简单有效。使用ANSYS软件对MRSI进行稳态热分析,以获得温度分布和传热速率,并通过模拟说明了柔性铜屏蔽条的必要性。在这个低温恒温器中,通过自制的光波驱动磁力显微镜获得了NdGaO(001)衬底上45nm厚的LaCaMnO薄膜在磁场下的形貌和磁畴图像。成像过程中的分辨率和噪声光谱揭示了整个低温恒温器的温度稳定性和低振动。在开发这种低温恒温器过程中获得的经验将有助于为各种需要使用低温温度的光学应用建立类似类型的低温恒温器。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d2ea/9964935/755db3dbfb27/micromachines-14-00378-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d2ea/9964935/b1ed9a12b221/micromachines-14-00378-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d2ea/9964935/8b352c3e9b1b/micromachines-14-00378-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d2ea/9964935/6c07691c97a6/micromachines-14-00378-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d2ea/9964935/b0e24f93b674/micromachines-14-00378-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d2ea/9964935/755db3dbfb27/micromachines-14-00378-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d2ea/9964935/b1ed9a12b221/micromachines-14-00378-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d2ea/9964935/8b352c3e9b1b/micromachines-14-00378-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d2ea/9964935/6c07691c97a6/micromachines-14-00378-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d2ea/9964935/b0e24f93b674/micromachines-14-00378-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d2ea/9964935/755db3dbfb27/micromachines-14-00378-g006.jpg

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本文引用的文献

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