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一种置于10特斯拉无液氦超导磁体中的压电可旋转磁力显微镜系统。

A piezoelectric rotatable magnetic force microscope system in a 10 T cryogen-free superconducting magnet.

作者信息

Xiang Kui, Hou Yubin, Wang Jihao, Zhang Jing, Feng Qiyuan, Wang Ze, Meng Wenjie, Lu Qingyou, Lu Yalin

机构信息

High Magnetic Field Laboratory, Hefei Institutes of Physical Science, Chinese Academy of Science, Hefei, Anhui 230031, China.

University of Science and Technology of China, Hefei, Anhui 230026, China.

出版信息

Rev Sci Instrum. 2022 Sep 1;93(9):093706. doi: 10.1063/5.0100662.

Abstract

We constructed a piezoelectric rotatable magnetic force microscope (MFM) that works in a 10 T cryogen-free superconducting magnet. The piezoelectric tube is deformed tangentially and drives a bearing under the inertial drive principle so the MFM head can obtain rotary movement. Due to the novel piezoelectric design, the MFM can be hung underneath the heat sink via a soft spring, and it can be rotated in a cryogen-free superconducting magnet so that the direction of the magnetic field can be changed from 0° to 90° continuously. The system functions in magnetic fields of up to 10 T in any direction relative to the tip-sample geometry. This is the first piezoelectric rotatable MFM ever reported. Using this homemade rotatable MFM, we imaged the structure of magnetic tracks on a commercial videotape. When the magnetic field angle changes from 0° to 90°, the magnetic moments on the tape and probe tip also rotate. A magnetic field strength of 0.8 T parallel to the sample surface is required to fully rotate the magnetic moment of the tip we used, but 0.8 T is not enough to fully rotate the magnetic moment of the sample. The piezoelectric rotatable MFM is expected to be widely used to study the anisotropy of magnetic materials due to its superiority in obtaining the same high field in and out of plane (compared with a vector magnet) as well as in maintaining the same scan area precisely (compared with a mechanical rotatable MFM, especially for atomic-scale scan areas).

摘要

我们构建了一种在10 T无液氦超导磁体中工作的压电旋转磁力显微镜(MFM)。压电管沿切线方向变形,并根据惯性驱动原理驱动一个轴承,从而使MFM探头能够获得旋转运动。由于采用了新颖的压电设计,该MFM可以通过软弹簧悬挂在散热器下方,并能在无液氦超导磁体中旋转,使得磁场方向能够在0°至90°之间连续变化。该系统在相对于针尖 - 样品几何结构的任何方向上,在高达10 T的磁场中均可正常工作。这是有史以来首次报道的压电旋转MFM。利用这种自制的旋转MFM,我们对商业录像带上的磁迹结构进行了成像。当磁场角度从0°变为90°时,磁带上的磁矩和探针针尖的磁矩也会旋转。要使我们所使用的针尖的磁矩完全旋转,需要平行于样品表面施加0.8 T的磁场强度,但0.8 T的磁场强度不足以使样品的磁矩完全旋转。由于压电旋转MFM在获得与矢量磁体相同的平面内和平面外高场方面以及在精确保持相同扫描区域方面(与机械旋转MFM相比,特别是对于原子尺度的扫描区域)具有优势,预计它将被广泛用于研究磁性材料的各向异性。

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