Schuh Benjamin, Issa Inas, Müller Timo, Kremmer Thomas, Gammer Christoph, Pippan Reinhard, Hohenwarter Anton
Erich-Schmid-Institute of Materials Science, Austrian Academy of Sciences, Jahnstraße 12, 8700 Leoben, Austria.
Department of Materials Science, Montanuniversität Leoben, Jahnstraße 12, 8700 Leoben, Austria.
Nanomaterials (Basel). 2023 Mar 2;13(5):924. doi: 10.3390/nano13050924.
A nanocrystalline CrMnFeCoNi high-entropy alloy produced using severe plastic deformation using high-pressure torsion was annealed at selected temperatures and times (450 °C for 1 h and 15 h and at 600 °C for 1 h), causing a phase decomposition into a multi-phase structure. The samples were subsequently deformed again by high-pressure torsion to investigate the possibility of tailoring a favorable composite architecture by re-distributing, fragmenting, or partially dissolving the additional intermetallic phases. While the second phase in the 450 °C annealing states had high stability against mechanical mixing, a partial dissolution could be achieved in the samples subjected to 600 °C for 1 h.
采用高压扭转严重塑性变形制备的纳米晶CrMnFeCoNi高熵合金在选定的温度和时间(450℃保温1小时和15小时以及600℃保温1小时)下进行退火,导致相分解成多相结构。随后,通过高压扭转使样品再次变形,以研究通过重新分布、破碎或部分溶解额外的金属间相来定制有利的复合结构的可能性。虽然在450℃退火状态下的第二相具有较高的抗机械混合稳定性,但在600℃保温1小时的样品中可以实现部分溶解。