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传统和超声振动辅助金刚石加工引起的锂硅玻璃陶瓷的边缘崩边损伤。

Edge chipping damage in lithium silicate glass-ceramics induced by conventional and ultrasonic vibration-assisted diamond machining.

机构信息

School of Electrical and Mechanical Engineering, The University of Adelaide, Adelaide 5005, SA, Australia.

Research Laboratory for Dental Biomaterials, Dental Clinic 1 - Operative Dentistry and Periodontology, University of Erlangen-Nuremberg, Erlangen, Germany.

出版信息

Dent Mater. 2023 Jun;39(6):557-567. doi: 10.1016/j.dental.2023.04.001. Epub 2023 Apr 18.

Abstract

OBJECTIVES

Diamond machining of lithium silicate glass-ceramics (LS) induces extensive edge chipping damage, detrimentally affecting LS restoration functionality and long-term performance. This study approached novel ultrasonic vibration-assisted machining of pre-crystallized and crystallized LS materials to investigate induced edge chipping damage in comparison with conventional machining.

METHODS

The vibration-assisted diamond machining was conducted using a five-axis ultrasonic high-speed grinding/machining machine at different vibration amplitudes while conventional machining was performed using the same machine without vibration assistance. LS microstructural characterization and phase development were performed using scanning electron microscopy (SEM) and x-ray diffraction (XRD) techniques. Machining-induced edge chipping depths, areas and morphology were also characterized using the SEM and Java-based imaging software.

RESULTS

All machining-induced edge chipping damages resulted from brittle fractures. The damage scales, however, depended on the material microstructures; mechanical properties associated with the fracture toughness, critical strain energy release rates, brittleness indices, and machinability indices; and ultrasonic vibration amplitudes. Pre-crystallized LS with more glass matrix and lithium metasilicate crystals yielded respective 1.8 and 1.6 times greater damage depths and specific damage areas than crystallized LS with less glass matrix and tri-crystal phases in conventional machining. Ultrasonic machining at optimized amplitudes diminished such damages by over 50 % in pre-crystallized LS and up to 13 % in crystallized LS.

SIGNIFICANCE

This research highlights that ultrasonic vibration assistance at optimized conditions may advance current dental CAD/CAM machining techniques by significant suppression of edge chipping damage in pre-crystallized LS.

摘要

目的

对锂硅玻璃陶瓷(LS)进行金刚石加工会导致广泛的边缘崩边损伤,从而对 LS 修复功能和长期性能产生不利影响。本研究采用新型超声振动辅助加工预析晶和结晶 LS 材料,以研究与传统加工相比所产生的边缘崩边损伤。

方法

在不同的振动幅度下,使用五轴超声高速磨削/加工机床进行振动辅助金刚石加工,而在没有振动辅助的情况下,使用相同的机床进行传统加工。采用扫描电子显微镜(SEM)和 X 射线衍射(XRD)技术对 LS 的微观结构特征和相演变进行了研究。还采用 SEM 和基于 Java 的成像软件对加工引起的边缘崩边深度、面积和形貌进行了表征。

结果

所有加工引起的边缘崩边损伤均源于脆性断裂。然而,损伤程度取决于材料的微观结构;与断裂韧性、临界应变能释放率、脆性指数和可加工性指数相关的机械性能;以及超声振动幅度。在传统加工中,具有更多玻璃基质和锂硅酸钠晶体的预析晶 LS 的损伤深度和比损伤面积分别比具有较少玻璃基质和三晶相的结晶 LS 大 1.8 倍和 1.6 倍。在优化的振幅下进行超声加工,可使预析晶 LS 的这种损伤减少 50%以上,结晶 LS 的损伤减少 13%。

意义

本研究表明,在优化条件下采用超声振动辅助可能会通过显著抑制预析晶 LS 的边缘崩边损伤,从而推进当前的牙科 CAD/CAM 加工技术。

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