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2
Bisphenol A release from orthodontic adhesives and its correlation with the degree of conversion.正畸粘结剂中双酚 A 的释放及其与转化率的相关性。
Am J Orthod Dentofacial Orthop. 2015 Jan;147(1):29-36. doi: 10.1016/j.ajodo.2014.09.013.
3
Bisphenol A release from an orthodontic adhesive and its correlation with the degree of conversion on varying light-curing tip distances.正畸胶粘剂中双酚 A 的释放及其与不同光固化尖端距离下转化率的关系。
Am J Orthod Dentofacial Orthop. 2011 Aug;140(2):239-44. doi: 10.1016/j.ajodo.2010.02.037.
4
Microleakage under orthodontic brackets bonded with the custom base indirect bonding technique.正畸托槽的微渗漏与定制基间接粘接技术。
Eur J Orthod. 2010 Jun;32(3):259-63. doi: 10.1093/ejo/cjp090. Epub 2009 Sep 13.
5
HPLC analysis of eluted monomers from two composite resins cured with LED and halogen curing lights.对用发光二极管（LED）和卤素固化灯固化的两种复合树脂洗脱单体进行高效液相色谱（HPLC）分析。
J Biomed Mater Res B Appl Biomater. 2009 Jan;88(1):191-6. doi: 10.1002/jbm.b.31167.
6
Evaluation of monomer leaching from a dual cured resin cement.双固化树脂水门汀中单体浸出的评估
J Biomed Mater Res B Appl Biomater. 2008 Aug;86(2):523-9. doi: 10.1002/jbm.b.31052.
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Systematic review of the chemical composition of contemporary dental adhesives.当代牙科粘合剂化学成分的系统评价。
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8
Assessment of bisphenol-A release from orthodontic adhesives.正畸粘合剂中双酚A释放量的评估。
Am J Orthod Dentofacial Orthop. 2007 Jan;131(1):72-5. doi: 10.1016/j.ajodo.2006.08.013.
9
HPLC analysis of components released from dental composites with different resin compositions using different extraction media.使用不同萃取介质对具有不同树脂成分的牙科复合材料释放的成分进行高效液相色谱分析。
J Mater Sci Mater Med. 2007 Jan;18(1):133-7. doi: 10.1007/s10856-006-0671-z.
10
Analysis of residual monomers in dendritic methacrylate copolymers and composites by HPLC and headspace-GC/MS.采用高效液相色谱法（HPLC）和顶空-气相色谱/质谱联用仪（headspace-GC/MS）分析树枝状甲基丙烯酸酯共聚物及复合材料中的残留单体。
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比较间接粘接剂释放的残留单体量。

Comparison of residual monomer amounts released from indirect bonding adhesives.

出版信息

Angle Orthod. 2023 Sep 1;93(5):558-565. doi: 10.2319/122322-864.1.

DOI:10.2319/122322-864.1
PMID:37212680
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC10575638/
Abstract

OBJECTIVES

To quantify the amount of residual monomer released from orthodontic adhesives used in the indirect bonding technique and compare it to a direct bonding composite resin.

MATERIALS AND METHODS

Five hundred stainless steel orthodontic brackets were bonded on bovine incisors using five groups of bonding resins: Transbond XT (TXT), Transbond Supreme LV (SLV), Sondhi Rapid-Set (SRS), Transbond IDB (IDB), and Custom I.Q. (CIQ). Liquid samples were gathered on the first, seventh, 21st, and 35th days. Residual monomer release was measured from the liquid samples with a liquid chromatography device. In addition, the amount and shape of the adhesive between the tooth surface and the bracket base was evaluated using obtained electron microscopy images. The data were analyzed using analysis of variance, and a Tukey post-hoc test was applied.

RESULTS

Hydroxyethylmethacrylate and bisphenol A-glycidyl methacrylate monomers were released by all study groups. Urethane-dimethacrylate was released from the TXT, SLV, IDB, and CIQ groups. Triethylene glycol dimethacrylate was released from TXT, SLV, IDB, and SRS groups. The amount of total monomer release was higher in chemically cured adhesives than in light-cured adhesives. Among the chemically cured adhesives, premix adhesives had the highest amount of total monomer release. The light-cured adhesives had less thickness.

CONCLUSIONS

Light-curing adhesives have significantly less monomer release than chemically polymerized adhesives.

摘要

目的

定量测定间接粘结技术中使用的正畸粘结剂释放的残留单体量，并与直接粘结复合树脂进行比较。

材料和方法

将 500 个不锈钢正畸托槽用 5 组粘结树脂粘结在牛切牙上：Transbond XT（TXT）、Transbond Supreme LV（SLV）、Sondhi Rapid-Set（SRS）、Transbond IDB（IDB）和 Custom I.Q.（CIQ）。第 1、7、21 和 35 天采集液体样本。用液相色谱仪测量液体样本中的残留单体释放量。此外，通过获得的电子显微镜图像评估牙面与托槽基底之间的粘结剂的数量和形状。使用方差分析对数据进行分析，并应用 Tukey 事后检验。

结果

所有研究组均释放出羟乙基甲基丙烯酸酯和双酚 A 缩水甘油甲基丙烯酸酯单体。TXT、SLV、IDB 和 CIQ 组释放出聚氨酯二甲基丙烯酸酯。TXT、SLV、IDB 和 SRS 组释放出三乙二醇二甲基丙烯酸酯。化学固化粘结剂释放的总单体量高于光固化粘结剂。在化学固化粘结剂中，预混粘结剂释放的总单体量最高。光固化粘结剂的厚度较小。

结论

光固化粘结剂释放的单体明显少于化学聚合粘结剂。