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激光粉末床熔融制备Inconel 718部件过程中层间冷却时间对孔隙率和熔池影响的研究

Study on the Effect of Inter-Layer Cooling Time on Porosity and Melt Pool in Inconel 718 Components Processed by Laser Powder Bed Fusion.

作者信息

Baldi Niccolò, Giorgetti Alessandro, Palladino Marco, Giovannetti Iacopo, Arcidiacono Gabriele, Citti Paolo

机构信息

Department of Engineering Science, Guglielmo Marconi University, 00193 Rome, Italy.

Department of Industrial, Electronic and Mechanical Engineering, Roma Tre University, 00146 Rome, Italy.

出版信息

Materials (Basel). 2023 May 24;16(11):3920. doi: 10.3390/ma16113920.

Abstract

This paper investigates the effects on the material microstructure of varying the Inter-Layer Cooling Time (ILCT) during the printing process in laser powder bed fusion (L-PBF) multi-laser machines. Despite these machines allowing higher productivity rates compared to single laser machines, they are affected by lower ILCT values, which could be critical for material printability and microstructure. The ILCT values depend both on the process parameter sets and design choices for the parts and play an important role in the Design for Additive Manufacturing approach in L-PBF process. In order to identify the critical range of ILCT for this working condition, an experimental campaign is presented on the nickel-based superalloy Inconel 718, which is widely used for the printing of turbomachinery components. The effect of ILCT on the microstructure of the material is evaluated in terms of porosity and melt pool analysis on printed cylinder specimens, considering ILCT decreasing and increasing in the range of 22 to 2 s. The experimental campaign shows that an ILCT of less than 6 s introduces criticality in the material microstructure. In particular, at an ILCT value of 2 s, widespread keyhole porosity (close to 1‱) and critical and deeper melt pool (about 200 microns depth) are measured. This variation in melt pool shape indicates a change in the powder melting regime and, consequently, modifications of the printability window promoting the expansion of the keyhole region. In addition, specimens with geometry obstructing the heat flow have been studied using the critical ILCT value (2 s) to evaluate the effect of the surface-to-volume ratio. The results show an enhancement of the porosity value (about 3‱), while this effect is limited for the depth of the melt pool.

摘要

本文研究了在激光粉末床熔融(L-PBF)多激光设备的打印过程中,改变层间冷却时间(ILCT)对材料微观结构的影响。尽管与单激光设备相比,这些设备能够实现更高的生产率,但它们受到较低ILCT值的影响,而ILCT值对于材料的可打印性和微观结构可能至关重要。ILCT值既取决于工艺参数集,也取决于零件的设计选择,并且在L-PBF工艺的增材制造设计方法中起着重要作用。为了确定这种工作条件下ILCT的临界范围,针对广泛用于涡轮机械部件打印的镍基高温合金Inconel 718开展了一项实验研究。通过对打印圆柱试样进行孔隙率和熔池分析,评估了ILCT在22至2秒范围内减小和增大时对材料微观结构的影响。实验研究表明,ILCT小于6秒会在材料微观结构中引入临界状态。特别是,当ILCT值为2秒时,测量到广泛存在的匙孔孔隙率(接近1‱)以及临界且更深的熔池(约200微米深)。熔池形状的这种变化表明粉末熔化状态发生了改变,进而促进了匙孔区域扩展的可打印性窗口的改变。此外,使用临界ILCT值(2秒)研究了具有阻碍热流几何形状的试样,以评估表面积与体积比的影响。结果显示孔隙率值有所增加(约3‱),而这种影响对熔池深度的影响有限。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fab3/10253632/30563993b012/materials-16-03920-g001.jpg

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