Department of Biological, Chemical, and Pharmaceutical Science and Technology (STEBICEF), University of Palermo, Palermo, Italy.
Department of Biomedical, Dental, Morphological and Functional Imaging Sciences, University of Messina, Via Consolare Valeria, 98125 Messina.
Nat Prod Res. 2024 May;38(10):1786-1792. doi: 10.1080/14786419.2023.2218974. Epub 2023 Jun 12.
Quality control of protein supplements intended for a large audience of consumers such as sportspeople is particularly important. A case study on quality control of dietary supplements containing protein and protein components is presented. The objective of the study was to evaluate the conformity of the quantities of amino acids, essential and branched-chain amino acids, declared on the label through measurements with chromatographic analytical tools. 16 sportspeople supplements from different European countries were tested. Analysis of concentrated whey protein highlighted some differences between the label and what was experimentally determined; in these samples some amino acids (6 amino acids out of 19) exceeded the maximum tolerance (>20%) regulated by the European Commission. To a lesser extent, analysis of the other classes revealed amino acid concentrations that exceeded the maximum analytical tolerance percentage. As regards the essential and branched amino acid supplements, it was seen that the declared quantity conforms with that determined experimentally.
对于面向广大消费者(如运动员)的蛋白质补充剂,质量控制尤为重要。本文介绍了一个关于含有蛋白质和蛋白质成分的膳食补充剂的质量控制案例研究。研究的目的是通过色谱分析工具的测量来评估标签上宣称的氨基酸、必需和支链氨基酸的数量的一致性。测试了来自不同欧洲国家的 16 种运动员补充剂。对浓缩乳清蛋白的分析显示出标签与实验确定值之间存在一些差异;在这些样品中,一些氨基酸(19 种中的 6 种)超过了欧盟规定的最大允许公差(>20%)。在分析其他类别时,发现氨基酸浓度超过了最大分析公差百分比。至于必需和支链氨基酸补充剂,发现宣称的数量与实验确定的数量相符。