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酸性饮料对玻璃离子水门汀和非玻璃离子水门汀大块充填材料的硬度、弹性模量和耐磨性的影响。

Effect of Acidic Beverages on the Hardness, Elastic Modulus and Wear Resistance of Giomer and Nongiomer Bulk-fill Materials.

机构信息

*Zeynep Batu Eken, DDS, Yeditepe University Faculty of Dentistry, Istanbul, Turkey.

Hiroyuki Miyajima, DDS, PhD, Department of Preventive and Restorative Sciences, School of Dental Medicine, University of Pennsylvania, Philadelphia, PA, USA.

出版信息

Oper Dent. 2023 Jul 1;48(4):435-446. doi: 10.2341/22-063-L.

Abstract

OBJECTIVES

The aim of this study was to evaluate and compare the effect of acidic beverages on the hardness, elastic modulus, and wear resistance of four different resin-based restorative materials.

METHODS AND MATERIALS

A total of 128 specimens (10 mm diameter, 4 mm thickness) were prepared from a conventional resin composite (Filtek Z250 [Z250]), a giomer bulk-fill (Beautifil Bulk Restorative [BBR]) and two nongiomer bulk-fill materials (Tetric N-Ceram Bulk Fill [TNC] and SonicFill 2 [SF2]). Each material group was divided into four subgroups (n=8) according to the storage media: artificial saliva (control), orange juice, regular Coke, and sports drink. The experimental specimens were immersed in the solutions for 30 minutes, five times a day for 5 days and kept in artificial saliva for an hour between the immersion periods. Control specimens were stored in artificial saliva for 5 days. The nanoindentation test with a Berkovich diamond tip was used to determine the hardness and elastic modulus before and after the 5-day storage periods. Following the nanoindentation tests, the specimens were subjected to a chewing simulator for 120,000 cycles. The specimens were then scanned with a three-dimensional scanner. The wear resistance was analyzed by measuring the volume and height loss. Specimens were observed by environmental scanning electron microscopy. The statistical analyses were performed by analysis of variance, Tukey HDS test, and paired samples t-test (α=0.05).

RESULTS

Z250 showed significantly higher elastic modulus in all groups (p<0.05). After erosive cycles, the greatest decrease in hardness and elastic modulus was observed for BBR. TNC showed higher wear resistance than the other resin-based materials (p<0.05). The BBR specimens immersed in acidic solutions showed higher wear rates than the artificial saliva group (p<0.05).

CONCLUSIONS

Conventional resin composite showed higher hardness and elastic modulus than bulk-fill materials when exposed to acidic beverages but comparable or lower wear resistance. Degradation due to acidic beverages most affected the mechanical properties of giomer bulk-fill.

摘要

目的

本研究旨在评估和比较酸性饮料对四种不同树脂基修复材料硬度、弹性模量和耐磨性的影响。

方法和材料

共制备 128 个试件(直径 10mm,厚度 4mm),来自传统树脂复合材料(Filtek Z250[Z250])、玻璃离子体大块充填材料(Beautifil Bulk Restorative[BBR])和两种非玻璃离子体大块充填材料(Tetric N-Ceram Bulk Fill[TNC]和 SonicFill 2[SF2])。根据储存介质,将每组材料分为 4 个亚组(n=8):人工唾液(对照)、橙汁、普通可乐和运动饮料。实验标本每天在溶液中浸泡 30 分钟,共 5 天,在浸泡期间每小时在人工唾液中保存 1 小时。对照组标本在人工唾液中储存 5 天。使用 Berkovich 金刚石压头进行纳米压痕试验,在 5 天储存期前后测定硬度和弹性模量。纳米压痕试验后,将试件在咀嚼模拟器上进行 120000 次循环。然后用三维扫描仪扫描试件。通过测量体积和高度损失来分析耐磨性。用环境扫描电子显微镜观察试件。采用方差分析、Tukey HDS 检验和配对样本 t 检验(α=0.05)进行统计分析。

结果

Z250 在所有组中均表现出明显较高的弹性模量(p<0.05)。经过侵蚀循环后,BBR 的硬度和弹性模量下降最大。TNC 显示出比其他树脂基材料更高的耐磨性(p<0.05)。在酸性溶液中浸泡的 BBR 试件的磨损率高于人工唾液组(p<0.05)。

结论

与大块充填材料相比,传统树脂复合材料在接触酸性饮料时表现出更高的硬度和弹性模量,但耐磨性相当或更低。酸性饮料的降解对玻璃离子体大块充填材料的力学性能影响最大。

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