Ghelbere Raluca, Ilie Nicoleta
Department of Conservative Dentistry and Periodontology, University Hospital, LMU, Germany.
Department of Conservative Dentistry and Periodontology, University Hospital, LMU, Germany.
J Mech Behav Biomed Mater. 2023 Aug;144:105982. doi: 10.1016/j.jmbbm.2023.105982. Epub 2023 Jun 18.
The present study aimed to assess the applicability of Orr's equation on light-cured resin-based composites (RBCs) tested in 3- and 4-point bending tests, as well as assess the operator reliability of this method.
Fracture mirrors of 320 specimens (n = 320) made of four RBCs that had failed in the two tests were analyzed microscopically and consequently two radii of each specimen were measured by two operators, each measuring twice. The mirror constant A was calculated using Orr's equation. The results of the two operators were compared using a t-Test and further assessment of the data was performed using a MANOVA, Tukey's post hoc test and regression analysis.
With the exception of 11 specimens, the measurement of the fracture mirror radii was carried out successfully. The calculation of the mirror constant proved successful with a high coefficient of determination (R > 0.98). The calculated mirror constants were operator-independent if the results of more than one measurement was taken into consideration. The ratio of the mirror constant A to the fracture toughness K lay between 2.1 and 2.4 for three of the four RBC. The fourth RBC had a ratio of 1.6 and was the only one where different mirror constants were observed as a function of the testing method.
The present study proves the applicability of brittle fracture mechanics on RBCs despite them often being regarded as not brittle due to their also plastic behavior.
本研究旨在评估奥尔方程在三点和四点弯曲试验中对光固化树脂基复合材料(RBC)的适用性,并评估该方法的操作者可靠性。
对在两项试验中失效的由四种RBC制成的320个试样(n = 320)的断裂镜面进行显微镜分析,随后由两名操作者测量每个试样的两个半径,每人测量两次。使用奥尔方程计算镜面常数A。使用t检验比较两名操作者的结果,并使用多变量方差分析、图基事后检验和回归分析对数据进行进一步评估。
除11个试样外,成功进行了断裂镜面半径的测量。镜面常数的计算证明是成功的,决定系数较高(R > 0.98)。如果考虑多次测量的结果,计算出的镜面常数与操作者无关。四种RBC中的三种,镜面常数A与断裂韧性K的比值在2.1至2.4之间。第四种RBC的比值为1.6,是唯一一种根据测试方法观察到不同镜面常数的材料。
本研究证明了脆性断裂力学在RBC上的适用性,尽管RBC由于其塑性行为通常不被视为脆性材料。