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采用现代空气喷砂技术、光动力疗法与传统金刚石砂片预处理对 PEEK 种植体与复合树脂的剪切粘结强度和表面粗糙度的调制作用。

Modulation of implants PEEK to composite resin shear bond strength and surface roughness on pre-treatment with contemporary air abrasion techniques vs photodynamic therapy vs conventional diamond grit bur.

机构信息

Department of O&MFS and Diagnostic Sciences, Faculty of Dentistry, Riyadh Elm University, Riyadh, Saudi Arabia.

Department of Oral and Craniofacial Sciences, Faculty of Dentistry, University of Malaya, Kuala Lumpur, Malaysia.

出版信息

Photodiagnosis Photodyn Ther. 2023 Sep;43:103689. doi: 10.1016/j.pdpdt.2023.103689. Epub 2023 Jul 4.

Abstract

AIM

The chief aim of the study was to determine/equate the surface roughness (SRa) and shear bond strength (BS) of pretreated PEEK discs with contemporary air abrasion techniques, photodynamic (PD) therapy by curcumin photosensitizer (PS) and conventional diamond grit straight fissure bur adhered to the composite resin discs.

MATERIAL AND METHOD

Two hundred discs of PEEK were prepared of 6 mm × 2 mm × 10 mm dimension. The discs were randomly divided into five groups (n = 40) for treatment, Group I: treatment with deionized distilled water (control group); Group II: PD therapy using curcumin PS; Group III: discs treated and abraded with air-borne particles (ABP) silica (30 μm particle size) modified alumina (Al); Group IV: ABP of alumina (110 μm particle size); and Group V: The PEEK were finished with 600-μm grit size straight diamond cutting bur installed in high speed hand-piece. The surface profilometer was used to evaluate the values of surface roughness (SRa) of pretreated PEEK discs. The discs were luted and bonded to discs of composite resin. The bonded PEEK samples were placed in Universal testing machine to evaluate shear BS. The type of BS failure for PEEK discs pre-treated with five regimes respectively was evaluated under stereo-microscope. The data was statistically analyzed using one-way ANOVA and the comparisons between mean values of shear BS were evaluated by Tukey's test (ρ≤0.05).

RESULTS

The PEEK samples pre-treated with diamond cutting straight fissure burs displayed statistically significant highest value of SRa values (3.258± 0.785 µm). Similarly, the shear BS was observed to be higher for the PEEK discs pre-treated with straight fissure bur (22.37±0.78 MPa). A comparable difference but not statistically significant difference was observed between PEEK discs pre-treated by curcumin PS and ABP-silica modified alumina (ρ ≥ 0.05).

CONCLUSION

PEEK discs pre-treated with diamond grit straight fissure bur displayed highest values of SRa and shear BS. It was trailed by ABP-Al pre-treated discs; whereas the SRa and shear BS values for the discs pre-treated with ABP-silica modified Al and curcumin PS did not show competitive difference.

摘要

目的

本研究的主要目的是确定/比较经预处理聚醚醚酮(PEEK)盘与现代空气喷砂技术、姜黄素光敏剂(PS)光动力(PD)治疗和复合树脂盘上附着的常规金刚石直裂钻的表面粗糙度(SRa)和剪切结合强度(BS)。

材料和方法

制备 6mm×2mm×10mm 尺寸的 PEEK 圆盘 200 个。将圆盘随机分为五组(n=40)进行处理,第 I 组:用去离子蒸馏水(对照组)处理;第 II 组:用姜黄素 PS 进行 PD 治疗;第 III 组:用空气传播的颗粒(ABP)硅(30μm 粒径)改性氧化铝(Al)处理和喷砂;第 IV 组:ABP 氧化铝(110μm 粒径);第 V 组:用安装在高速手持器械上的 600μm 粒度直金刚石切割钻对 PEEK 进行精加工。使用表面轮廓仪评估预处理 PEEK 盘的表面粗糙度(SRa)值。将圆盘胶合并粘接到复合树脂盘上。将粘合的 PEEK 样品放置在万能试验机中以评估剪切 BS。在立体显微镜下评估分别用五种方案预处理的 PEEK 盘的 BS 失效类型。使用单向方差分析对数据进行统计分析,并用 Tukey 检验评估剪切 BS 平均值之间的比较(ρ≤0.05)。

结果

用金刚石直裂钻预处理的 PEEK 样品显示出统计学上最高的 SRa 值(3.258±0.785μm)。同样,用直裂钻预处理的 PEEK 盘的剪切 BS 较高(22.37±0.78MPa)。用姜黄素 PS 和 ABP-改性硅氧化铝预处理的 PEEK 盘之间观察到类似的差异,但无统计学意义(ρ≥0.05)。

结论

用金刚石磨料直裂钻预处理的 PEEK 盘显示出最高的 SRa 和剪切 BS 值。其次是 ABP-Al 预处理的圆盘;而用 ABP-改性硅氧化铝和姜黄素 PS 预处理的圆盘的 SRa 和剪切 BS 值没有显示出竞争差异。

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