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白鸡蛋壳粉对富钙混合物抗压强度、水溶性和凝结时间的影响

Effects of White Chicken Eggshell Powder on Compressive Strength, Water Solubility, and Setting Time of Calcium-Enriched Mixture.

作者信息

Sedigh-Shams Mahdi, Nabavizadeh Mohammadreza, Jafari Elham

机构信息

Department of Endodontics, School of Dentistry, Shiraz University of Medical Sciences, Shiraz, Fars, Iran.

Oral and Dental Disease Research Center, Department of Endodontics, School of Dentistry, Shiraz University of Medical Sciences, Shiraz, Fars, Iran.

出版信息

Iran Endod J. 2023;18(3):152-158. doi: 10.22037/iej.v18i3.39798.

Abstract

INTRODUCTION

The present study aimed to evaluate the effects of adding chicken eggshell powder (CESP) to calcium-enriched mixture (CEM) cement on its compressive strength (CS), solubility, and setting time.

MATERIALS AND METHODS

In this study, CESP was added at weight percentages of 3% and 5% to the powder component of the CEM cement. To measure the CS, a total of 36 samples (height, 6 mm; diameter, 4 mm) were tested in a universal testing machine. The setting time was assessed for 18 disk-shaped samples (diameter, 10 mm; height, 1 mm). Additionally, solubility test was performed on 18 samples (diameter, 8 mm; height, 1 mm) after 24 hours, 72 hours, seven days, and 14 days under dehydration conditions by calculating the weight changes; the results were then subjected to a normality test. Next, for the comparison of different test groups, parametric ANOVA test and post-hoc Tukey's multiple comparison test were performed at a significance level of 0.05.

RESULTS

The addition of 5% CESP to the CEM cement significantly reduced its setting time and water solubility (=0.02 and =0.01, respectively). Moreover, it significantly increased the CS over a 21-day period (<0.001). Additionally, the addition of 3% CESP also resulted in a significant increase in CS (<0.001). While 3% CESP reduced setting time and water solubility, the difference was not statistically significant.

CONCLUSION

The findings suggest that the addition of 5% CESP to CEM cement has the potential to improve its sealing ability, durability, and ability to withstand chewing forces in endodontic treatments. These results highlight the relevance of CESP as an additive for cement modifications and indicate its potential clinical implications.

摘要

引言

本研究旨在评估向富钙混合物(CEM)水泥中添加鸡蛋壳粉(CESP)对其抗压强度(CS)、溶解度和凝结时间的影响。

材料与方法

在本研究中,将CESP按重量百分比3%和5%添加到CEM水泥的粉末成分中。为测量CS,共36个样本(高度6mm;直径4mm)在万能试验机上进行测试。对18个圆盘形样本(直径10mm;高度1mm)评估凝结时间。此外,在脱水条件下,分别于24小时、72小时、7天和14天后,对18个样本(直径8mm;高度1mm)进行溶解度测试,通过计算重量变化得出结果,然后对结果进行正态性检验。接下来,为比较不同测试组,在显著性水平0.05下进行参数方差分析测试和事后Tukey多重比较测试。

结果

向CEM水泥中添加5%的CESP显著缩短了其凝结时间并降低了水溶性(分别为=0.02和=0.01)。此外,在21天内显著提高了CS(<0.001)。另外,添加3%的CESP也导致CS显著增加(<0.001)。虽然3%的CESP降低了凝结时间和水溶性,但差异无统计学意义。

结论

研究结果表明,向CEM水泥中添加5%的CESP有可能提高其在根管治疗中的密封能力、耐久性和承受咀嚼力的能力。这些结果突出了CESP作为水泥改性添加剂的相关性,并表明了其潜在的临床意义。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6275/10329759/443360f274b9/IEJ-18-152-g001.jpg

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