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用于测定水 - 二甲基亚砜二元混合物中二甲亚砜浓度的微波传感器。

Microwave Sensor for the Determination of DMSO Concentration in Water-DMSO Binary Mixture.

作者信息

Harnsoongnoen Supakorn, Buranrat Benjaporn

机构信息

The Biomimicry for Sustainable Agriculture, Health, Environment and Energy Research Unit, Department of Physics, Faculty of Science, Mahasarakham University, Kantarawichai District, Maha Sarakham 44150, Thailand.

Faculty of Medicine, Mahasarakham University, Muang District, Maha Sarakham 44000, Thailand.

出版信息

Micromachines (Basel). 2023 Jul 5;14(7):1378. doi: 10.3390/mi14071378.

Abstract

This research aims to develop a microwave sensor to accurately measure the concentration of dimethyl sulfoxide (DMSO) in water-DMSO binary mixtures. The proposed sensor will utilize microwave frequency measurements to determine the DMSO concentration, providing a non-invasive and efficient method for analyzing DMSO solutions. The research will involve the design, fabrication, and testing of the sensor, as well as the development of an appropriate calibration model. The outcomes of this study will contribute to improved monitoring and quality control in various fields, including pharmaceuticals, chemical synthesis, and biomedical research. The binary mixtures of dimethyl sulfoxide (DMSO) and water with varying concentrations were investigated in the frequency range of 1 GHz to 5 GHz at room temperature using a microwave sensor. The proposed microwave sensor design was based on an interdigital capacitor (IDC) microstrip antenna loaded with a hexagonal complementary ring resonator (HCRR). The performance of the sensor, fabricated using the print circuit board (PCB) technique, was validated through simulations and experiments. The reflection coefficient (S) and resonance frequency (F) of binary mixtures of DMSO and water solutions were recorded and analyzed for DMSO concentrations ranging from 0% / to 75% /. Mathematical models were developed to analyze the data, and laboratory tests showed that the sensor can detect levels of DMSO/water binary mixtures. The sensor is capable of detecting DMSO concentrations ranging from 0% / to 75% /, with a maximum sensitivity of 0.138 dB/% for S and ΔS and 0.2 MHz/% for F and ΔF at a concentration of 50% /. The developed microwave sensor can serve as an alternative for detecting DMSO concentrations in water using a simple and cost-effective technique. This method can effectively analyze a wide range of concentrations, including highly concentrated solutions, quickly and easily.

摘要

本研究旨在开发一种微波传感器,以精确测量水 - 二甲基亚砜(DMSO)二元混合物中二甲基亚砜的浓度。所提出的传感器将利用微波频率测量来确定DMSO浓度,为分析DMSO溶液提供一种非侵入性且高效的方法。该研究将涉及传感器的设计、制造和测试,以及开发合适的校准模型。本研究的成果将有助于改善制药、化学合成和生物医学研究等各个领域的监测和质量控制。在室温下,使用微波传感器在1 GHz至5 GHz的频率范围内研究了不同浓度的二甲基亚砜(DMSO)和水的二元混合物。所提出的微波传感器设计基于加载有六边形互补环谐振器(HCRR)的叉指电容器(IDC)微带天线。使用印刷电路板(PCB)技术制造的传感器性能通过模拟和实验得到验证。记录并分析了DMSO和水溶液二元混合物的反射系数(S)和共振频率(F),以确定DMSO浓度范围为0%至75%。开发了数学模型来分析数据,实验室测试表明该传感器可以检测DMSO/水二元混合物的浓度水平。该传感器能够检测0%至75%的DMSO浓度,在50%的浓度下,S和ΔS的最大灵敏度为0.138 dB/%,F和ΔF的最大灵敏度为0.2 MHz/%。所开发的微波传感器可以作为一种使用简单且经济高效的技术检测水中DMSO浓度的替代方法。该方法可以快速、轻松地有效分析包括高浓度溶液在内的广泛浓度范围。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/04e1/10383328/b7fbfb69b6a8/micromachines-14-01378-g001.jpg

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