Institute of Advanced Materials and School of Chemistry and Chemical Engineering, Southeast University, Nanjing, 211189, China.
Institute of Advanced Materials and School of Chemistry and Chemical Engineering, Southeast University, Nanjing, 211189, China.
STAR Protoc. 2023 Sep 15;4(3):102488. doi: 10.1016/j.xpro.2023.102488. Epub 2023 Jul 28.
Here, we present a protocol for the construction of a hierarchical host-guest supramolecular self-assembly system in water. We describe steps for determining the binding levels and capturing the morphologies of hierarchical self-assembly. We detail procedures for using UV-vis spectra, nuclear magnetic resonance spectra, scanning electron microscopy, and transmission electron microscopy for the assembly. This protocol is useful for analyzing the detailed chemical structure and morphological variation of hierarchical host-guest supramolecular self-assembly systems. For complete details on the use and execution of this protocol, please refer to Chen et al. (2022)..
在这里,我们提出了一种在水中构建分级主客体超分子自组装体系的方案。我们描述了确定结合水平和捕获分级自组装形态的步骤。我们详细介绍了使用紫外-可见光谱、核磁共振谱、扫描电子显微镜和透射电子显微镜进行组装的过程。该方案有助于分析分级主客体超分子自组装体系的详细化学结构和形态变化。如需了解本方案的使用和实施的完整详细信息,请参考 Chen 等人(2022 年)。