用于解析无阳极电池中电解质分解反应的定量核磁共振协议。
Protocol for quantitative nuclear magnetic resonance for deciphering electrolyte decomposition reactions in anode-free batteries.
机构信息
Beijing Key Laboratory of Green Chemical Reaction Engineering and Technology, Department of Chemical Engineering, Tsinghua University, Beijing 100084, China.
Advanced Research Institute for Multidisciplinary Science, Beijing Institute of Technology, Beijing 100081, China; School of Materials Science and Engineering, Beijing Institute of Technology, Beijing 100081, China.
出版信息
STAR Protoc. 2022 Dec 16;3(4):101867. doi: 10.1016/j.xpro.2022.101867. Epub 2022 Nov 19.
In this protocol, we describe the quantification of electrolytes using nuclear magnetic resonance. We detail the steps involved for battery cycling, sample preparation, instrument operation, and data analysis. The protocol can be used to quantify electrolyte decomposition reactions and the apparent electron transfer numbers of different electrolyte components. The protocol is optimized for lithium-based anode-free batteries but can also be applied to other rechargeable batteries. For complete details on the use and execution of this protocol, please refer to Zhou et al. (2022)..
在本方案中，我们描述了使用核磁共振定量分析电解质。我们详细说明了电池循环、样品制备、仪器操作和数据分析的步骤。该方案可用于定量分析电解质分解反应和不同电解质成分的表观电子转移数。该方案针对无锂阳极电池进行了优化，但也可应用于其他可充电电池。如需了解本方案的使用和执行的完整详细信息，请参考 Zhou 等人（2022 年）。
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