Department of Process and Food Engineering, Faculty of Engineering, Universiti Putra Malaysia, 43400 Serdang, Selangor, Malaysia.
Department of Process and Food Engineering, Faculty of Engineering, Universiti Putra Malaysia, 43400 Serdang, Selangor, Malaysia; Laboratory of Halal Services, Halal Products Research Institute, Putra Infoport, Universiti Putra Malaysia, 43400 Serdang, Selangor, Malaysia.
Int J Biol Macromol. 2023 Nov 1;251:126212. doi: 10.1016/j.ijbiomac.2023.126212. Epub 2023 Aug 9.
The present study developed the formulation of active bionanocomposites films endowed with the abilities of high biodegradability and antimicrobials for active packaging applications. The aim of this work was to prepare poly (lactic acid)/poly (butylene succinate) (PLA/PBS) blended films reinforced with different concentrations of nanofibrillated cellulose (NFC) and 9 % of thymol essential oil (EO) using the casting method. The active films were further evaluated through Fourier transform infrared spectroscopy (FTIR); as well as mechanical, physical, water vapour permeability (WVP), thermal analysis (TGA), biodegradation, morphological, and antimicrobial (% reduction of bacteria) testing. The tensile strength (TS) of PLA/PBS blend films increased by 12 % with the incorporation of 2 wt% of NFC. The PLA/PBS/NFC with 9 % thymol EO has a good water barrier performance with its tensile strength, elongation at break, and tensile modulus was 13.2 MPa, 13.1 %, and 513 MPa respectively. The presence of NFC promoted the disintegration of PLA/PBS films by 70.5 %. These films promoted the antibacterial activity against S. aureus and E. coli. The study demonstrates that the developed films improved the qualities of chicken fillets and have great potential to be used as active bionanocomposites in food packaging applications.
本研究开发了具有高生物降解性和抗菌能力的活性生物纳米复合材料薄膜配方,用于活性包装应用。这项工作的目的是使用浇铸法制备不同浓度纳米原纤纤维素(NFC)增强的聚乳酸/聚丁二酸丁二醇酯(PLA/PBS)共混薄膜,并添加 9%的百里香精油(EO)。通过傅里叶变换红外光谱(FTIR)、机械性能、物理性能、水蒸气透过率(WVP)、热分析(TGA)、生物降解性、形态学和抗菌性(细菌减少百分比)测试进一步评估了活性薄膜。随着 2wt%NFC 的加入,PLA/PBS 共混薄膜的拉伸强度(TS)提高了 12%。含有 9%百里香精油的 PLA/PBS/NFC 具有良好的水分阻隔性能,其拉伸强度、断裂伸长率和拉伸模量分别为 13.2MPa、13.1%和 513MPa。NFC 的存在促进了 PLA/PBS 薄膜的崩解,达到 70.5%。这些薄膜对金黄色葡萄球菌和大肠杆菌表现出抗菌活性。研究表明,所开发的薄膜改善了鸡肉的品质,在食品包装应用中具有很大的潜力作为活性生物纳米复合材料。