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一种用于测量液相声速的双路径脉冲回波仪器及对二甲苯和四种卤代烯烃制冷剂[R1234yf、R1234ze(E)、R1233zd(E)和R1336mzz(Z)]的测量

A Dual-Path Pulse-Echo Instrument for Liquid-Phase Speed of Sound and Measurements on -Xylene and Four Halogenated-Olefin Refrigerants [R1234yf, R1234ze(E), R1233zd(E), and R1336mzz(Z)].

作者信息

McLinden Mark O, Perkins Richard A

机构信息

Applied Chemicals and Materials Division, National Institute of Standards and Technology, 325 Broadway, Mailstop 647.08, Boulder, Colorado 80305, United States.

出版信息

Ind Eng Chem Res. 2023 Jul 28;62(31):12381-12406. doi: 10.1021/acs.iecr.3c01720. eCollection 2023 Aug 9.

DOI:10.1021/acs.iecr.3c01720
PMID:37576937
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC10416216/
Abstract

We describe an instrument to measure the speed of sound in liquids based on the dual-path, pulse-echo technique; it covers a temperature range of 228.15-423.15 K, with pressures of up to 93 MPa. It differs from similar instruments in the method of mounting the quartz-crystal transducer, a path-length ratio of 2.5:1, and automated data-collection protocols. The path-length difference was calibrated with measurements on high-purity propane. The performance of the instrument was verified by comparison with recent literature data on -xylene. We present new liquid-phase measurements for the halogenated-olefin refrigerants 2,3,3,3-tetrafluoroprop-1-ene [R1234yf], -1,3,3,3-tetrafluoroprop-1-ene [R1234ze(E)], -1-chloro-3,3,3-trifluoroprop-1-ene [R1233zd(E)], and -1,1,1,4,4,4-hexafluorobut-2-ene [R1336mzz(Z)]. These measurements cover a combined temperature range of 230 to 420 K, with pressures of up to 50 MPa; these data are compared to literature data (where available) and multiproperty equations of state. The average relative expanded uncertainty in the speed of sound ranged from 0.035 to 0.088% for the different fluids.

摘要

我们描述了一种基于双路径脉冲回波技术测量液体中声速的仪器；其温度范围为228.15 - 423.15 K，压力高达93 MPa。它在石英晶体换能器的安装方法、路径长度比为2.5:1以及自动数据采集协议方面与类似仪器不同。路径长度差通过对高纯度丙烷的测量进行校准。通过与近期关于对二甲苯的文献数据比较，验证了该仪器的性能。我们给出了卤代烯烃制冷剂2,3,3,3 - 四氟丙烯[R1234yf]、1,3,3,3 - 四氟丙烯[R1234ze(E)]、1 - 氯 - 3,3,3 - 三氟丙烯[R1233zd(E)]和1,1,1,4,4,4 - 六氟 - 2 - 丁烯[R1336mzz(Z)]的新的液相测量结果。这些测量覆盖的温度范围为230至420 K，压力高达50 MPa；将这些数据与文献数据（若有）以及多性质状态方程进行了比较。对于不同流体，声速的平均相对扩展不确定度范围为0.

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9a37/10416216/20f5e4694c6c/ie3c01720_0019.jpg
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