Academic Department of Food (DAALM), Technological Federal University of Parana, Londrina, Brazil.
Department of Civil, Chemical and Environmental Engineering (DICCA), University of Genoa, Genoa, Italy.
Nat Prod Res. 2024 Oct;38(19):3311-3320. doi: 10.1080/14786419.2023.2244133. Epub 2023 Aug 10.
Due to the high content of phenolics and anthocyanins of L. tea and the sensibility of these bioactive compounds, this work aimed to optimize the obtention of microcapsules by spray-drying, using inulin as a carrier agent. Using a Box-Behnken Design, the effects of inlet temperature (130, 150, and 170 °C), feed flow rate (5, 10, and 15 mL min), and inulin concentration (5, 10, and 15 g L) were evaluated. It was possible to obtain pale-rose, slightly sweet instant powders with good total polyphenol content (1.12 mg g) and anthocyanins encapsulation efficiency (32.3-60.6%), besides moisture (4.61-17.79%) and water activity (0.221-0.501), indicating physico-chemical and microbiological stability of the microcapsules. A simultaneous optimization with the desirability function was performed to maximize all the response variables analyzed, and the optimum conditions of 5 g L of inulin, inlet temperature of 170 °C, and feed flow rate of 83 mL min were found.
由于 L.茶含有丰富的酚类化合物和花青素,并且这些生物活性化合物很敏感,因此本工作旨在通过喷雾干燥优化微胶囊的获得,使用菊粉作为载体。使用 Box-Behnken 设计,评估了入口温度(130、150 和 170°C)、进料流速(5、10 和 15 mL min)和菊粉浓度(5、10 和 15 g L)的影响。可以获得淡玫瑰色、略带甜味的即时粉末,具有良好的总多酚含量(1.12 mg g)和花青素包封效率(32.3-60.6%),此外还有水分(4.61-17.79%)和水分活度(0.221-0.501),表明微胶囊具有物理化学和微生物稳定性。使用理想函数进行了同时优化,以最大化分析的所有响应变量,发现最佳条件为菊粉浓度 5 g L、入口温度 170°C 和进料流速 83 mL min。