State Key Laboratory of Food Science and Resources, Jiangnan University, Wuxi 214122, China.
Shandong Food Ferment Industry Research & Design Institute, Qilu University of Technology, Jinan 250013, China.
Food Res Int. 2023 Oct;172:113118. doi: 10.1016/j.foodres.2023.113118. Epub 2023 Jun 12.
Water-in-oil (W/O) emulsion is promising to design fat-reduced foods for 3D printing. In this study, oleogel-based W/O emulsion containing 65% water fraction was prepared by sunflower wax (SW, 1.0 wt%) and soybean phosphatidylethanolamine (SP, 0.5 wt%) with stability exceeding 30 days. Besides reducing interfacial tension, from X-ray diffraction and rheological results, SP was considered co-oleogelator to change the crystal habit of SW to enhance the external SW-based oleogel structure. The strong external oleogel structure was not only good for reducing droplets movements to improve physical stability, but facilitating the molding and supporting abilities of the emulsion gel in 3D printing. Based on rheological measurements, the emulsion gels were shown improved printing performance with SP increasing: extrusion (shear-thinning behavior), recovery (excellent thixotropy), and self-supporting (sufficient storage modulus and deformation resistance). In 3D printing, the emulsion gels with growing SP were displayed better shape retention and allowed printing the designs with more delicate and vivid features. This study provided new insight for W/O emulsion formation using natural ingredients for 3D printing to create fat-reduced foods.
水包油(W/O)乳液有望设计用于 3D 打印的低脂食品。在这项研究中,通过使用葵花蜡(SW,1.0wt%)和大豆磷脂酰乙醇胺(SP,0.5wt%)制备了含有 65%水相分数的基于油凝胶的 W/O 乳液,其稳定性超过 30 天。除了降低界面张力外,从 X 射线衍射和流变学结果来看,SP 被认为是共油凝胶剂,它改变了 SW 的晶体习性,从而增强了 SW 基外部油凝胶结构。强大的外部油凝胶结构不仅有利于减少液滴的运动,从而提高物理稳定性,而且有利于乳液凝胶在 3D 打印中的成型和支撑能力。基于流变学测量,随着 SP 的增加,乳液凝胶表现出改善的打印性能:挤出(剪切变稀行为)、恢复(出色的触变性)和自支撑(足够的储能模量和变形阻力)。在 3D 打印中,随着 SP 增加的乳液凝胶具有更好的形状保持性,并允许打印具有更精细和生动特征的设计。这项研究为使用天然成分形成 W/O 乳液以创建低脂食品用于 3D 打印提供了新的见解。