猪脂肪组织中雄烯酮的定量测定
Quantitative determination of androstenone in pig adipose tissue.
作者信息
De Brabander H F, Verbeke R
出版信息
J Chromatogr. 1986 Aug 29;363(2):293-302. doi: 10.1016/s0021-9673(01)83748-1.
PMID:3771689
Abstract
A simple, cheap and rapid method for the quantitative determination of the boar taint substance, 5 alpha-androst-16-en-3-one, in pig adipose tissue is described. After saponification of the fat the androstenone is extracted, derivatised with o-(pentafluorobenzyl)hydroxylamine hydrochloride in pyridine and analysed by fused-silica open-tubular capillary gas chromatography with electron-capture detection.
摘要
描述了一种用于定量测定猪脂肪组织中雄烯酮（一种公猪异味物质，即5α-雄甾-16-烯-3-酮）的简单、廉价且快速的方法。脂肪皂化后，提取雄烯酮，用盐酸邻（五氟苄基）羟胺在吡啶中进行衍生化，然后通过带有电子捕获检测的熔融石英开管毛细管气相色谱法进行分析。
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