De Brabander H F, Verbeke R
J Chromatogr. 1986 Aug 29;363(2):293-302. doi: 10.1016/s0021-9673(01)83748-1.
A simple, cheap and rapid method for the quantitative determination of the boar taint substance, 5 alpha-androst-16-en-3-one, in pig adipose tissue is described. After saponification of the fat the androstenone is extracted, derivatised with o-(pentafluorobenzyl)hydroxylamine hydrochloride in pyridine and analysed by fused-silica open-tubular capillary gas chromatography with electron-capture detection.