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当代种植体基台螺钉的表面、微观结构及力学特性

Surface, microstructural and mechanical characterization of contemporary implant abutment screws.

作者信息

Kouveliotis George, Dimitriadis Konstantinos, Kourtis Stefanos, Zinelis Spiros

机构信息

Department of Prosthodontics, School of Dentistry, National and Kapodistrian University of Athens, Athens, Greece.

Department of Biomaterials, School of Dentistry, National and Kapodistrian University of Athens, Athens, Greece.

出版信息

Dent Mater. 2024 Feb;40(2):219-226. doi: 10.1016/j.dental.2023.11.002. Epub 2023 Nov 15.

Abstract

OBJECTIVES

The aim of the present work was to evaluate six commercially available abutment screws by characterising roughness parameters, microstructure and mechanical properties.

METHODS

Six abutment screws from each implant system, were used. The surface roughness parameters (S, S, S, S, S, S and S) were identified by an optical interferometric profiler. Microstructural observations and crystallographic analysis were performed using a scanning electron microscope (SEM) equipped with an energy dispersive X-ray spectroscopy (EDX) device for elemental analysis and an X-ray diffractometer (XRD), respectively. The Martens Hardness (HM), Indentation Modulus (E), elastic index (η) and Vickers hardness (HV) of all specimens were determined by instrumented indentation testing (IIT). The results were analyzed by one-way ANOVA and Tukey multiple-comparison tests (a=0.05).

RESULTS

EDX and XRD showed the abutment screws to be mixed α- and β-phase titanium alloys. Microstructural analysis revealed a fine homogeneous microstructure without porosity, consisting of fine dispersoid rods of β-phase embedded in a continuous α-phase matrix. Statistically significant differences were found among the mechanical properies and surface roughness parameters apart from S, S and S.

CONCLUSIONS

The tested abutment screws showed significant differences in the probed properties, and, thus, differences in their clinical behaviour are anticipated.

摘要

目的

本研究的目的是通过表征粗糙度参数、微观结构和力学性能来评估六种市售基台螺钉。

方法

使用来自每个种植系统的六枚基台螺钉。通过光学干涉轮廓仪确定表面粗糙度参数(S、S、S、S、S、S和S)。分别使用配备有用于元素分析的能量色散X射线光谱仪(EDX)装置的扫描电子显微镜(SEM)和X射线衍射仪(XRD)进行微观结构观察和晶体学分析。通过仪器化压痕测试(IIT)测定所有试样的马氏体硬度(HM)、压痕模量(E)、弹性指数(η)和维氏硬度(HV)。结果通过单因素方差分析和Tukey多重比较检验进行分析(α=0.05)。

结果

EDX和XRD显示基台螺钉为α相和β相混合钛合金。微观结构分析显示出精细均匀的微观结构,无孔隙,由嵌入连续α相基体中的β相精细弥散棒组成。除了S、S和S之外,在力学性能和表面粗糙度参数之间发现了统计学上的显著差异。

结论

测试的基台螺钉在所探测的性能方面表现出显著差异,因此,可以预期它们在临床行为上也存在差异。

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