Department of Restorative Dentistry, Dental Sciences Research Center, School of Dentistry, Guilan University of Medical Sciences, Rasht, Iran.
Dental Sciences Research Center, School of Dentistry, Guilan University of Medical Sciences, Rasht, Iran.
Dent Med Probl. 2023 Oct-Dec;60(4):641-647. doi: 10.17219/dmp/151945.
The long-term mechanical properties and stability of various resin composites in areas under stress are questionable.
The aim of the study was to determine the effects of long-term hydrothermal aging on the mechanical properties of a microhybrid conventional resin composite and its bulk-fill counterpart.
We used a conventional and high-viscosity restorative bulk-fill resin-based composites (RBCs) from one company. Bar-shaped specimens of each type of resin composite were fabricated using steel molds and divided into 2 groups. The specimens were stored at 37°C for 24 h, and half of the specimens in each group were subjected to the 3-point bending flexural test and microhardness measurement. The remaining specimens were aged for 10,000 thermal cycles between 5°C and 55°C, and then subjected to flexural testing and microhardness measurement. A Vickers microhardness tester was used to estimate the surface microhardness of the specimens. Data was analyzed using an independent t test and the Mann-Whitney U test. The statistical significance level was set at p ≤ 0.05. Scanning electron microscopy (SEM) was used to investigate the surface of each material.
The bulk-fill RBC showed similar flexural strength and modulus to its conventional counterpart before aging. The flexural strength of both resin composites was significantly decreased after thermocycling (p < 0.001). Hydrothermal aging had no significant effects on the flexural modulus (p = 0.84). There was a significant decrease in the surface microhardness of the bulk-fill RBC. Scanning electron microscopy photomicrographs showed several pits as a result of the exfoliation of the filler particles on the surface of the bulk-fill RBC after aging.
The flexural strength of both resin composites decreased significantly after aging. The flexural properties, surface changes and microhardness of the bulk-fill type were additionally affected by the aging process.
各种处于压力下的树脂复合材料的长期机械性能和稳定性存在疑问。
本研究旨在确定长期水热老化对一种微混合常规树脂复合材料及其块状填充对应物的机械性能的影响。
我们使用了来自同一家公司的一种常规和高粘度的修复性块状填充树脂基复合材料(RBC)。使用钢模具制造每种类型的树脂复合材料的条形试件,并将其分为两组。将试件在 37°C 下储存 24 小时,每组的一半试件进行三点弯曲挠曲试验和显微硬度测量。其余试件在 5°C 和 55°C 之间进行 10000 次热循环老化,然后进行弯曲试验和显微硬度测量。使用维氏显微硬度计估计试件的表面显微硬度。使用独立 t 检验和曼-惠特尼 U 检验分析数据。统计显著性水平设置为 p ≤ 0.05。使用扫描电子显微镜(SEM)研究每种材料的表面。
块状填充 RBC 在老化前表现出与常规对照材料相似的弯曲强度和模量。两种树脂复合材料的弯曲强度在热循环后均显著降低(p < 0.001)。水热老化对弯曲模量没有显著影响(p = 0.84)。块状填充 RBC 的表面显微硬度显著降低。扫描电子显微镜照片显示,老化后块状填充 RBC 表面的填料颗粒发生剥落,导致出现多个凹坑。
两种树脂复合材料的弯曲强度在老化后均显著降低。块状填充类型的弯曲性能、表面变化和显微硬度还受到老化过程的影响。