Fujian Key Laboratory of Oral Diseases & Fujian Provincial Engineering Research Center of Oral Biomaterial & Stomatological Key Laboratory of Fujian College and University, School and Hospital of Stomatology, Fujian Medical University, China; Department of Prosthodontics & Research Center of Dental Esthetics and Biomechanics, Fujian Medical University, China.
Fujian Key Laboratory of Oral Diseases & Fujian Provincial Engineering Research Center of Oral Biomaterial & Stomatological Key Laboratory of Fujian College and University, School and Hospital of Stomatology, Fujian Medical University, China; Department of Prosthodontics & Research Center of Dental Esthetics and Biomechanics, Fujian Medical University, China.
J Mech Behav Biomed Mater. 2024 Mar;151:106331. doi: 10.1016/j.jmbbm.2023.106331. Epub 2023 Dec 20.
This in vitro study aimed to determine the optimal frequency and energy settings for debonding zirconia restorations using an erbium-doped yttrium aluminum garnet (Er:YAG) laser. A total of 200 zirconia specimens (5 mm × 5 mm × 1.5 mm) were fabricated from two types of materials: (1) 3 mol% yttria oxide stabilized tetragonal zirconia polycrystalline (3Y-TZP) and (2) 5 mol% yttria oxide stabilized tetragonal zirconia polycrystalline (5Y-TZP). The zirconia specimens were bonded to dentin using resin cement (RelyX Ultimate, 3 M) and divided into 20 groups based on their laser treatments (n = 5). Er:YAG laser treatment was applied at various frequencies (10 Hz and 20 Hz) and energies (80 mJ, 100 mJ, 120 mJ, 140 mJ, 160 mJ, 180 mJ, 200 mJ, 220 mJ, 240 mJ, and 260 mJ). The time required to debond the specimens and the temperature changes that dentin underwent during the laser treatment were recorded. The surface morphologies of the debonded dentin and zirconia specimens were observed using scanning electron microscopy (SEM). Additional zirconia specimens were fabricated for 4-point flexural strength testing and surface roughness measurements. Statistical analyses were conducted using three-way analysis of variance (ANOVA) and Student-Newman-Keuls (SNK)-q tests (α = 0.05). The debonding time of each specimen varied between 4.8 and 160.4 s, with an average value of 59.2 s. The dentin temperature change for each specimen ranged from 2.3 to 3.6 °C, with an average value of 2.7 °C. The debonding time was significantly influenced by the zirconia material type and laser energy, but it was not affected by the laser frequency. Among the specimens, those made of 3Y-TZP needed significantly more time for debonding than 5Y-TZP. The optimal energies were 220 mJ for 3Y-TZP and 200 mJ for 5Y-TZP. The laser frequency, laser energy, and type of zirconia material had no effect on the dentin temperature change. Additionally, no surface alternations were observed on the dentin or zirconia materials after laser treatment. The surface roughness and flexural strength of the zirconia materials remained unchanged after laser treatment. In summary, Er:YAG laser treatment effectively and safely removes zirconia restorations without impacting their mechanical properties, with a safe temperature change of less than 5.6 °C. The optimum frequency and energy settings for debonding 3Y-TZP and 5Y-TZP restorations were found to be 10/20 Hz and 220 mJ and 10/20 Hz and 200 mJ, respectively.
本体外研究旨在确定使用掺铒钇铝石榴石(Er:YAG)激光去除氧化锆修复体的最佳频率和能量设置。总共制备了 200 个氧化锆标本(5mm×5mm×1.5mm),分为两种材料:(1)3mol%氧化钇稳定四方氧化锆多晶(3Y-TZP)和(2)5mol%氧化钇稳定四方氧化锆多晶(5Y-TZP)。使用树脂水泥(RelyX Ultimate,3M)将氧化锆标本粘结到牙本质上,并根据激光处理将其分为 20 组(n=5)。以不同的频率(10Hz 和 20Hz)和能量(80mJ、100mJ、120mJ、140mJ、160mJ、180mJ、200mJ、220mJ、240mJ 和 260mJ)对 Er:YAG 激光进行处理。记录分离标本所需的时间和激光处理过程中牙本质的温度变化。使用扫描电子显微镜(SEM)观察分离的牙本质和氧化锆标本的表面形态。为四点弯曲强度测试和表面粗糙度测量制备了额外的氧化锆标本。使用三因素方差分析(ANOVA)和 Student-Newman-Keuls(SNK)-q 检验(α=0.05)进行统计分析。每个标本的分离时间在 4.8 秒至 160.4 秒之间,平均值为 59.2 秒。每个标本的牙本质温度变化范围为 2.3°C 至 3.6°C,平均值为 2.7°C。分离时间受氧化锆材料类型和激光能量的显著影响,但不受激光频率的影响。在标本中,3Y-TZP 比 5Y-TZP 需要更长的分离时间。最佳能量分别为 3Y-TZP 的 220mJ 和 5Y-TZP 的 200mJ。激光频率、激光能量和氧化锆材料类型对牙本质温度变化没有影响。此外,激光处理后牙本质或氧化锆材料表面未见任何变化。激光处理后氧化锆材料的表面粗糙度和弯曲强度保持不变。总之,Er:YAG 激光治疗可有效、安全地去除氧化锆修复体,而不会影响其机械性能,温度变化安全,低于 5.6°C。发现分离 3Y-TZP 和 5Y-TZP 修复体的最佳频率和能量设置分别为 10/20Hz 和 220mJ,以及 10/20Hz 和 200mJ。