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铣削与熔融沉积成型打印氧化锆的抗弯强度、抗弯模量和显微硬度;常规与高速烧结的影响。

Flexural strength, flexural modulus and microhardness of milled vs. fused deposition modeling printed Zirconia; effect of conventional vs. speed sintering.

机构信息

Department of Restorative Dentistry, Faculty of Dentistry, King Abdulaziz University, Jeddah, Saudi Arabia.

Advanced Technology Dental Research Laboratory, King Abdulaziz University, P.O. Box 80209, Jeddah, 21589, Saudi Arabia.

出版信息

BMC Oral Health. 2024 Jan 7;24(1):38. doi: 10.1186/s12903-023-03829-8.

Abstract

BACKGROUND

Various methods can be used for creating zirconia dental restorations, including 3-dimensional (3D) printing and computer-aided design/ computer-aided manufacturing (CAD/CAM) milling. The fused deposition modeling (FDM) printing method for zirconia presents numerous advantages, albeit research on the mechanical properties of these materials and resultant restorations remains scarce. Such developments are undeniably intriguing and warrant further investigation. The objective of the present study was to evaluate the impact of the sintering firing cycle (Conventional vs. Speed sintering) on the flexural strength, flexural modulus, and Vickers Microhardness of milled vs. FDM printed zirconia.

METHODS

A total of 60 bars (2 × 5 × 27 mm) were fabricated for flexural strength testing, along with 40 discs (12 × 1.5 mm) for Vickers microhardness testing. Half of the specimens underwent conventional sintering, while the other half underwent a speed sintering cycle. The flexural strength and modulus were determined by a three-point bending test in a universal testing machine. The microhardness of the specimens was evaluated using a Vickers microhardness tester. Statistical analysis was performed using a two-way ANOVA test with a post-hoc Tukey test (p < 0.05).

RESULTS

CAD/CAM milled zirconia had significantly higher flexural strength and modulus than FDM-printed zirconia. The sintering process did not significantly affect the flexural strength or modulus of milled or FDM-printed zirconia. The milled speed sintering group had significantly higher values in the Vickers microhardness test compared to the other groups.

CONCLUSIONS

The mechanical properties of FDM-printed zirconia specimens were not found to be comparable to those of milled zirconia. Speed sintering cycle may produce milled zirconia restorations with similar flexural strength and modulus to conventional sintering, and even higher Vickers Microhardness values.

摘要

背景

各种方法可用于制作氧化锆牙科修复体,包括三维(3D)打印和计算机辅助设计/计算机辅助制造(CAD/CAM)铣削。熔融沉积建模(FDM)打印方法制作氧化锆具有许多优势,尽管对这些材料的机械性能及其修复体的研究仍然很少。这些发展无疑令人感兴趣,值得进一步研究。本研究的目的是评估烧结烧制周期(常规与快速烧结)对铣削与 FDM 打印氧化锆的抗弯强度、抗弯模量和维氏显微硬度的影响。

方法

共制作了 60 个(2×5×27mm)棒材用于抗弯强度测试,40 个(12×1.5mm)圆盘用于维氏显微硬度测试。一半的样本进行常规烧结,另一半进行快速烧结循环。抗弯强度和模量通过万能试验机的三点弯曲试验确定。使用维氏显微硬度计评估试样的显微硬度。采用双因素方差分析和事后 Tukey 检验(p<0.05)进行统计分析。

结果

CAD/CAM 铣削氧化锆的抗弯强度和模量明显高于 FDM 打印氧化锆。烧结过程对铣削或 FDM 打印氧化锆的抗弯强度或模量没有显著影响。与其他组相比,铣削快速烧结组在维氏显微硬度测试中具有更高的值。

结论

FDM 打印氧化锆试样的机械性能与铣削氧化锆不相当。快速烧结循环可能会产生与常规烧结相似的抗弯强度和模量,甚至更高维氏显微硬度值的铣削氧化锆修复体。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/eb9d/10771678/a78004c52fb2/12903_2023_3829_Fig1_HTML.jpg

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