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一种高热负荷下低温冷却硅晶体单色仪的热变形优化方法

A thermal deformation optimization method for cryogenically cooled silicon crystal monochromators under high heat load.

作者信息

Liu Jiayin, Ji Zhan, Fan Yichen, Yan Xinxin, Wang Miaomiao, Qin Hongliang

机构信息

Synchrotron Radiation Facility, Institute of Advanced Science Facilities, Guangming, Shenzhen, Guangdong 518107, People's Republic of China.

出版信息

J Synchrotron Radiat. 2024 Mar 1;31(Pt 2):260-267. doi: 10.1107/S1600577523010664. Epub 2024 Jan 22.

DOI:10.1107/S1600577523010664
PMID:38252523
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC10914174/
Abstract

A method to optimize the thermal deformation of an indirectly cryo-cooled silicon crystal monochromator exposed to intense X-rays at a low-emittance diffraction-limited synchrotron radiation source is presented. The thermal-induced slope error of the monochromator crystal has been studied as a function of heat transfer efficiency, crystal temperature distribution and beam footprint size. A partial cooling method is proposed, which flattens the crystal surface profile within the beam footprint by modifying the cooling contact area to optimize the crystal peak temperature. The optimal temperature varies with different photon energies, which is investigated, and a proper cooling strategy is obtained to fulfil the thermal distortion requirements over the entire photon energy range. At an absorbed power up to 300 W with a maximum power density of 44.8 W mm normal incidence beam from an in-vacuum undulator, the crystal thermal distortion does not exceed 0.3 µrad at 8.33 keV. This method will provide references for the monochromator design on diffraction-limited synchrotron radiation or free-electron laser light sources.

摘要

提出了一种优化间接低温冷却硅晶体单色仪热变形的方法,该单色仪在低发射度衍射极限同步辐射源下暴露于强X射线中。研究了单色仪晶体的热致斜率误差与传热效率、晶体温度分布和束斑尺寸的关系。提出了一种局部冷却方法,通过改变冷却接触面积来优化晶体峰值温度,从而使束斑内的晶体表面轮廓变平。研究了最佳温度随不同光子能量的变化情况,并获得了一种合适的冷却策略,以满足整个光子能量范围内的热畸变要求。在来自真空型波荡器的垂直入射光束吸收功率高达300 W、最大功率密度为44.8 W mm的情况下,在8.33 keV时晶体热畸变不超过0.3 µrad。该方法将为衍射极限同步辐射或自由电子激光光源的单色仪设计提供参考。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/826f/10914174/3968d6e5b088/s-31-00260-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/826f/10914174/f5a3115224e0/s-31-00260-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/826f/10914174/3968d6e5b088/s-31-00260-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/826f/10914174/f5a3115224e0/s-31-00260-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/826f/10914174/3968d6e5b088/s-31-00260-fig2.jpg

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本文引用的文献

1
Towards a wavefront-preservation X-ray crystal monochromator for high-repetition-rate FELs.面向高重复率 FEL 的波前保持型 X 射线晶体单色器。
J Synchrotron Radiat. 2023 Jul 1;30(Pt 4):686-694. doi: 10.1107/S1600577523004216. Epub 2023 Jun 15.
2
Cryo-cooled silicon crystal monochromators: a study of power load, temperature and deformation.低温冷却硅晶体单色仪:功率负载、温度及变形研究
J Synchrotron Radiat. 2022 Mar 1;29(Pt 2):377-385. doi: 10.1107/S160057752200039X. Epub 2022 Feb 8.
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Application of interference fits on cylindrical monochromator crystals to overcome clamping and cooling deformations.
J Synchrotron Radiat. 2019 Mar 1;26(Pt 2):382-385. doi: 10.1107/S1600577519001061. Epub 2019 Feb 12.
4
New challenges in beamline instrumentation for the ESRF Upgrade Programme Phase II.欧洲同步辐射装置升级计划第二阶段光束线仪器面临的新挑战。
J Synchrotron Radiat. 2014 Sep;21(Pt 5):986-95. doi: 10.1107/S1600577514015951. Epub 2014 Aug 29.
5
Diffraction-limited storage rings - a window to the science of tomorrow.衍射极限存储环——通往明日科学的一扇窗口。
J Synchrotron Radiat. 2014 Sep;21(Pt 5):837-42. doi: 10.1107/S1600577514019286. Epub 2014 Aug 31.
6
Anisotropic elasticity of silicon and its application to the modelling of X-ray optics.硅的各向异性弹性及其在X射线光学建模中的应用。
J Synchrotron Radiat. 2014 May;21(Pt 3):507-17. doi: 10.1107/S1600577514004962. Epub 2014 Apr 4.
7
Thermal deformation of cryogenically cooled silicon crystals under intense X-ray beams: measurement and finite-element predictions of the surface shape.强 X 射线束下深冷硅晶体的热变形:表面形状的测量和有限元预测。
J Synchrotron Radiat. 2013 Jul;20(Pt 4):567-80. doi: 10.1107/S0909049513009436. Epub 2013 May 8.
8
SHADOW3: a new version of the synchrotron X-ray optics modelling package.SHADOW3:一个新的同步加速器 X 射线光学建模包版本。
J Synchrotron Radiat. 2011 Sep;18(Pt 5):708-16. doi: 10.1107/S0909049511026306. Epub 2011 Jul 20.
9
Performance limits of direct cryogenically cooled silicon monochromators - experimental results at the APS.直接低温冷却硅单色仪的性能极限——美国阿贡国家实验室先进光子源的实验结果
J Synchrotron Radiat. 2000 Jan 1;7(Pt 1):12-7. doi: 10.1107/S0909049599014478.
10
The performance of a cryogenically cooled monochromator for an in-vacuum undulator beamline.用于真空型波荡器光束线的低温冷却单色仪的性能。
J Synchrotron Radiat. 2003 Jul 1;10(Pt 4):313-9. doi: 10.1107/s0909049503012135. Epub 2003 Jun 24.