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喷砂处理对表面形貌和结晶相的改变提高了铌酸钇稳定四方氧化锆多晶的弯曲和剪切结合强度。

Topographical and crystalline change on surface by sandblasting improve flexural and shear bond strength of niobia-modified yttria-stabilized tetragonal zirconia polycrystal.

机构信息

Department of Prosthodontics, Seoul National University School of Dentistry.

Department of Prosthodontics, School of Dentistry and Dental Research Institute, Seoul National University.

出版信息

Dent Mater J. 2024 Mar 29;43(2):216-226. doi: 10.4012/dmj.2023-225. Epub 2024 Feb 29.

Abstract

This study aimed to investigate the effects of sandblasting on the physical properties and bond strength of two types of translucent zirconia: niobium-oxide-containing yttria-stabilized tetragonal zirconia polycrystals ((Y, Nb)-TZP) and 5 mol% yttria-partially stabilized zirconia (5Y-PSZ). Fully sintered disc specimens were either sandblasted with 125 µm alumina particles or left as-sintered. Surface roughness, crystal phase compositions, and surface morphology were explored. Biaxial flexural strength (n=10) and shear bond strength (SBS) (n=12) were evaluated, including thermocycling conditions. Results indicated a decrease in flexural strength of 5Y-PSZ from 601 to 303 MPa upon sandblasting, while (Y, Nb)-TZP improved from 458 to 544 MPa. Both materials significantly increased SBS after sandblasting (p<0.001). After thermocycling, (Y, Nb)-TZP maintained superior SBS (14.3 MPa) compared to 5Y-PSZ (11.3 MPa) (p<0.001). The study concludes that (Y, Nb)-TZP is preferable for sandblasting applications, particularly for achieving durable bonding without compromising flexural strength.

摘要

本研究旨在探讨喷砂处理对两种半透明氧化锆的物理性能和粘结强度的影响

铌掺杂氧化钇稳定四方氧化锆多晶陶瓷((Y, Nb)-TZP)和 5mol%氧化钇部分稳定氧化锆(5Y-PSZ)。完全烧结的圆盘试件经过 125µm 氧化铝颗粒喷砂处理或保持烧结状态。研究了表面粗糙度、晶体相组成和表面形貌。评估了双轴弯曲强度(n=10)和剪切粘结强度(SBS)(n=12),包括热循环条件。结果表明,喷砂处理使 5Y-PSZ 的弯曲强度从 601MPa 降至 303MPa,而(Y, Nb)-TZP 则从 458MPa 提高至 544MPa。两种材料的 SBS 均显著提高(p<0.001)。经过热循环后,(Y, Nb)-TZP 的 SBS(14.3MPa)仍优于 5Y-PSZ(11.3MPa)(p<0.001)。研究结论认为,(Y, Nb)-TZP 更适合喷砂处理应用,特别是在不影响弯曲强度的情况下实现持久粘结。

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