Department of Prosthodontics, Seoul National University School of Dentistry.
Department of Prosthodontics, School of Dentistry and Dental Research Institute, Seoul National University.
Dent Mater J. 2024 Mar 29;43(2):216-226. doi: 10.4012/dmj.2023-225. Epub 2024 Feb 29.
This study aimed to investigate the effects of sandblasting on the physical properties and bond strength of two types of translucent zirconia: niobium-oxide-containing yttria-stabilized tetragonal zirconia polycrystals ((Y, Nb)-TZP) and 5 mol% yttria-partially stabilized zirconia (5Y-PSZ). Fully sintered disc specimens were either sandblasted with 125 µm alumina particles or left as-sintered. Surface roughness, crystal phase compositions, and surface morphology were explored. Biaxial flexural strength (n=10) and shear bond strength (SBS) (n=12) were evaluated, including thermocycling conditions. Results indicated a decrease in flexural strength of 5Y-PSZ from 601 to 303 MPa upon sandblasting, while (Y, Nb)-TZP improved from 458 to 544 MPa. Both materials significantly increased SBS after sandblasting (p<0.001). After thermocycling, (Y, Nb)-TZP maintained superior SBS (14.3 MPa) compared to 5Y-PSZ (11.3 MPa) (p<0.001). The study concludes that (Y, Nb)-TZP is preferable for sandblasting applications, particularly for achieving durable bonding without compromising flexural strength.
铌掺杂氧化钇稳定四方氧化锆多晶陶瓷((Y, Nb)-TZP)和 5mol%氧化钇部分稳定氧化锆(5Y-PSZ)。完全烧结的圆盘试件经过 125µm 氧化铝颗粒喷砂处理或保持烧结状态。研究了表面粗糙度、晶体相组成和表面形貌。评估了双轴弯曲强度(n=10)和剪切粘结强度(SBS)(n=12),包括热循环条件。结果表明,喷砂处理使 5Y-PSZ 的弯曲强度从 601MPa 降至 303MPa,而(Y, Nb)-TZP 则从 458MPa 提高至 544MPa。两种材料的 SBS 均显著提高(p<0.001)。经过热循环后,(Y, Nb)-TZP 的 SBS(14.3MPa)仍优于 5Y-PSZ(11.3MPa)(p<0.001)。研究结论认为,(Y, Nb)-TZP 更适合喷砂处理应用,特别是在不影响弯曲强度的情况下实现持久粘结。