Rajeev Rheya, Ramírez Aguilera Andrés, Marica Florea, Romero-Zerón Laura, Balcom Bruce J
UNB MRI Centre, Department of Physics, University of New Brunswick, Fredericton, New Brunswick, E3B 5A3, Canada; Department of Chemical Engineering, University of New Brunswick, Fredericton, NB E3B 5A3, Canada.
UNB MRI Centre, Department of Physics, University of New Brunswick, Fredericton, New Brunswick, E3B 5A3, Canada.
J Magn Reson. 2024 Mar;360:107637. doi: 10.1016/j.jmr.2024.107637. Epub 2024 Feb 14.
Fast Spin Echo MRI is now widely employed in biomedicine for proton density and T contrast imaging. Fast Spin Echo methods provide rapid data acquisition by employing multiple echoes to determine multiple k-space lines with single excitations. Due to the multi-exponential behavior of T in typical porous media, and the strong dependence of T on the details of the experiment, acquiring a proton density image with Fast Spin Echo methods requires favorable sample and acquisition parameters. In recent years, we have shown the value of pure phase encode Free Induction Decay based methods such as SPRITE. However, in a reservoir rock, a typical T* is hundreds of µs, whereas a typical T is hundreds of ms. Hence, there is merit in considering spin echo-based MRI measurements such as the Fast Spin Echo for rock core plug studies. A variable field superconducting magnet was employed in this study. This is a new class of magnet for MR/MRI. These magnets have the flexibility of operation in the field range of 0.01 Tesla to 3 Tesla. This is advantageous when working with rock core plugs, as it allows one to maximize sample magnetization, by increasing the static field while controlling magnetic susceptibility mismatch effects, and thereby T and T*, through reducing the static field. The magnetic fields employed in the study were 0.79, 1.5, and 3 Tesla. Measurements were undertaken on five brine-saturated reservoir rock core plugs (Bentheimer, Berea, Buff Berea, Nugget, and Wallace). The results show that Fast Spin Echo measurements are more sensitive than SPRITE methods in amenable samples and usually feature higher resolution. Quantification of saturation with Fast Spin Echo methods requires correction for T attenuation. The results also show that 3 Tesla is too high a static field in general for rock core MRI studies with either method. While the current study is focused on five representative reservoir rock cores, the conclusions which result are general for MRI of fluids in porous media.
快速自旋回波磁共振成像(Fast Spin Echo MRI)如今在生物医学中被广泛用于质子密度和T对比度成像。快速自旋回波方法通过利用多个回波在单次激发下确定多条k空间线来实现快速数据采集。由于典型多孔介质中T的多指数行为,以及T对实验细节的强烈依赖性,使用快速自旋回波方法获取质子密度图像需要合适的样品和采集参数。近年来,我们已经展示了基于纯相位编码自由感应衰减的方法(如SPRITE)的价值。然而,在储层岩石中,典型的T为数百微秒,而典型的T为数百毫秒。因此,考虑基于自旋回波的磁共振成像测量方法(如快速自旋回波)用于岩芯塞研究是有价值的。本研究中使用了可变场超导磁体。这是一类新型的用于磁共振/磁共振成像的磁体。这些磁体在0.01特斯拉至3特斯拉的场强范围内具有操作灵活性。这在处理岩芯塞时是有利的,因为它允许通过增加静磁场同时控制磁化率失配效应来最大化样品磁化强度,从而通过降低静磁场来控制T和T。研究中使用的磁场强度为0.79、1.5和3特斯拉。对五个盐水饱和的储层岩石岩芯塞(本特海默、贝雷亚、布夫贝雷亚、块金和华莱士)进行了测量。结果表明,在合适的样品中,快速自旋回波测量比SPRITE方法更灵敏,并且通常具有更高的分辨率。使用快速自旋回波方法对饱和度进行定量需要对T衰减进行校正。结果还表明,一般来说,对于使用这两种方法进行的岩芯磁共振成像研究,3特斯拉的静磁场过高。虽然当前研究集中在五个代表性的储层岩石岩芯上,但所得出的结论对于多孔介质中流体的磁共振成像具有普遍意义。