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电子背散射衍射(EBSD)对增材制造TiC-Fe基金属陶瓷微观结构和微观织构演变的研究——多次激光扫描的影响

EBSD investigation of microstructure and microtexture evolution on additively manufactured TiC-Fe based cermets-Influence of multiple laser scanning.

作者信息

Maurya H S, Vikram R J, Kumar R, Rahmani R, Juhani K, Sergejev F, Prashanth K G

机构信息

Department of Mechanical and Industrial Engineering, Tallinn University of Technology, Ehitajate tee 5, Tallinn 19086, Estonia; Luleå University of Technology, Department of Engineering Sciences and Mathematics, Luleå SE-97187, Sweden.

Department of Materials Engineering, Indian Institute of Science, Bangalore 560012, India.

出版信息

Micron. 2024 May;180:103613. doi: 10.1016/j.micron.2024.103613. Epub 2024 Feb 23.

Abstract

Sustainable TiC-Fe-based cermets have been fabricated by adopting an Additive Manufacturing route based on laser powder bed fusion technology (L-PBF). The objective is to produce crack-free cermet components by employing novel multiple laser scanning techniques with variations in laser process parameters. Electron backscatter diffraction analysis (EBSD) was used to study the microstructure and microtexture evolution with variations in laser process parameters. The investigation revealed that adjusting the preheating scan speed (PHS) and melting scan speed (MS) influenced the growth and nucleation of TiC phases. Lowering these speeds resulted in grain coarsening, while higher scan speeds led to grain refinement with larger sub-grain boundaries. Moreover, a high scanning speed increases the degree of dislocation density and internal stress in the fabricated cermet parts. Notably, it is revealed that decreasing the laser scan speed enhanced the proportion of high-angle grain boundaries in the cermet components, signifying an increase in material ductility.

摘要

通过采用基于激光粉末床熔融技术(L-PBF)的增材制造路线,制备了可持续的TiC-Fe基金属陶瓷。目的是通过采用具有不同激光工艺参数的新型多激光扫描技术来生产无裂纹的金属陶瓷部件。利用电子背散射衍射分析(EBSD)研究了随着激光工艺参数的变化,微观结构和微观织构的演变。研究表明,调整预热扫描速度(PHS)和熔化扫描速度(MS)会影响TiC相的生长和形核。降低这些速度会导致晶粒粗化,而较高的扫描速度会导致具有较大亚晶界的晶粒细化。此外,高扫描速度会增加所制备金属陶瓷部件中的位错密度和内应力。值得注意的是,研究发现降低激光扫描速度会提高金属陶瓷部件中高角度晶界的比例,这意味着材料延展性的增加。

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