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高应力水平下304不锈钢的蠕变变形与时效强化行为研究

Investigation on Creep Deformation and Age Strengthening Behavior of 304 Stainless Steel under High Stress Levels.

作者信息

Zhan Lihua, Xie Hao, Yang Youliang, Zhao Shuai, Chang Zhilong, Xia Yunni, Zheng Zeyu, Zhou Yujie

机构信息

Research Institute of Light Alloy, Central South University, Changsha 410083, China.

State Key Laboratory of Precision Manufacturing for Extreme Service Performance, Central South University, Changsha 410083, China.

出版信息

Materials (Basel). 2024 Jan 28;17(3):642. doi: 10.3390/ma17030642.

Abstract

The creep deformation behavior and age strengthening behavior of 304 stainless steel under high stress levels were systematically studied by uniaxial creep test, tensile test, XRD diffraction test and transmission electron microscopy. The results show that the total creep strain and the initial creep strain rate increase with the increase in stress level, and the creep strain in the whole aging process is mainly produced in the initial creep stage. The calculated stress exponent shows that the main mechanism of creep deformation of 304 stainless steel at 453 K is dislocation slip. The strength and plasticity of 304 stainless steel after creep aging are improved simultaneously. Microstructural observations indicate an increase in dislocation density and martensite content, as well as austenite and twins, leading to an improvement in strength and plasticity, respectively. In addition, considering the influence of dislocation density on creep behavior, the relative dislocation density increase is introduced into the hyperbolic sine creep model, and a simple mechanism-based creep aging constitutive model is established. The creep strain predicted by the model is in good agreement with the experimental data of 304 stainless steel. The findings can provide theoretical support for the application of creep age forming in 304 stainless steel parts.

摘要

通过单轴蠕变试验、拉伸试验、XRD衍射试验和透射电子显微镜,系统研究了304不锈钢在高应力水平下的蠕变变形行为和时效强化行为。结果表明,总蠕变应变和初始蠕变应变速率随应力水平的增加而增加,且整个时效过程中的蠕变应变主要产生在初始蠕变阶段。计算得到的应力指数表明,453K下304不锈钢蠕变变形的主要机制是位错滑移。蠕变时效后304不锈钢的强度和塑性同时提高。微观结构观察表明,位错密度、马氏体含量以及奥氏体和孪晶增加,分别导致强度和塑性提高。此外,考虑到位错密度对蠕变行为的影响,将相对位错密度增量引入双曲正弦蠕变模型,建立了一个基于简单机制的蠕变时效本构模型。该模型预测的蠕变应变与304不锈钢的实验数据吻合良好。研究结果可为304不锈钢零件蠕变时效成形的应用提供理论支持。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d84a/10856003/71578edaefb3/materials-17-00642-g001.jpg

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