Restorative Dental Sciences Department, College of Dentistry, King Saud University, Riyadh, Saudi Arabia.
Microsc Res Tech. 2024 Sep;87(9):2043-2052. doi: 10.1002/jemt.24584. Epub 2024 Apr 22.
Evaluation of the impact of the latest root canal disinfectant, that is carbon quantum dots (CQDs), synchronized microbubble-photodynamic activation (SYMPA), and Nd: YAG laser along with ethylenediaminetetraacetic acid (EDTA) as a final irrigant on the Marten hardness (MH), smear layer (SL) removal, and extrusion bond strength (EBS) of zirconia post to the canal dentin. Eighty intact single-rooted premolars were obtained and disinfected using 0.5% chloramine-T solution. Root canal preparation was performed using ProTaper files followed by obturation. The post space was prepared for prefabricated zirconia post and all the teeth were randomly divided into four groups based on the disinfection used (n = 20 each) Group 1: 5.25% NaOCl + 17% EDTA (Control), Group 2: Nd: YAG laser + 17% EDTA, Group 3: SYMPA + 17% EDTA, and Group 4: CQDs + 17% EDTA. MH, SL removal, and EBS of zirconia post-bonded to root dentin were performed using a microhardness tester, scanning electron microscope (SEM), and universal testing machine, respectively. Both intragroup and intergroup comparisons were performed using one-way analysis of variance (ANOVA) and posthoc-Tukey test for significant difference (p < .05). Group 2 samples (Nd: YAG laser + 17% EDTA) (0.24 ± 0.06 GPa) exhibited highest values of MH. Samples in group 3 (SYMPA + 17% EDTA) treated teeth unveiled the lowest MH scores (0.13 ± 0.02 GPa). Moreover, the coronal third of Group 3 specimens (SYMPA and 17% EDTA) (1.54 ± 0.31) eliminated SL from the canal with the greatest efficacy as well as presented the highest EBS (10.13 ± 0.69 MPa). However, the apical third of Group 1 samples (5.25% NaOCl + 17% EDTA) (2.95 ± 0.33) exhibited the least efficient elimination of SL from the radicular dentin as well as the lowest bond strength (5.11 ± 0.19 MPa) of zirconia post to the dentin. The SYMPA technique with 17% EDTA proved highly effective in removing the SL from canal dentin and enhancing the EBS of zirconia posts. The least preferable method for SL removal and MH improvement was found to be 5.25% NaOCl + 17% EDTA. CQDs and Nd: YAG laser demonstrated satisfactory smear layer removal properties from the canal, along with achieving appropriate bond strength of zirconia posts. RESEARCH HIGHLIGHTS: Nd: YAG laser and 17% EDTA as canal disinfectant exhibited the highest values of MH. Specimens irrigated with SYMPA and 17% EDTA eliminated SL from the canal with the greatest efficacy. The coronal third of Group 3 (SYMPA + 17% EDTA) samples unveiled the highest zirconia post-bond integrity score to the canal dentin. Cohesive failure was a dominant failure type among different experimental groups.
评估最新根管消毒剂——碳量子点(CQDs)、同步微泡光动力激活(SYMPA)联合钕:钇铝石榴石(Nd: YAG)激光与乙二胺四乙酸(EDTA)作为最终冲洗液对氧化锆桩与根管牙本质之间马滕硬度(MH)、玷污层(SL)去除和挤出结合强度(EBS)的影响。获得 80 颗完整的单根前磨牙,并用 0.5%氯胺-T 溶液消毒。使用 ProTaper 文件进行根管预备,然后进行充填。为预制氧化锆桩预备桩道,所有牙齿根据使用的消毒方法随机分为四组(每组 20 颗):第 1 组:5.25%次氯酸钠+17% EDTA(对照);第 2 组:Nd: YAG 激光+17% EDTA;第 3 组:SYMPA+17% EDTA;第 4 组:CQDs+17% EDTA。使用显微硬度计、扫描电子显微镜(SEM)和万能试验机分别检测氧化锆桩与根管牙本质结合后的 MH、SL 去除率和 EBS。采用单因素方差分析(ANOVA)和事后 Tukey 检验进行组内和组间比较,差异有统计学意义(p<.05)。第 2 组(Nd: YAG 激光+17% EDTA)样本(0.24±0.06 GPa)的 MH 值最高。第 3 组(SYMPA+17% EDTA)处理组的样本 MH 评分最低(0.13±0.02 GPa)。此外,第 3 组(SYMPA 和 17% EDTA)样本的冠部(0.13±0.02 GPa)最有效地去除了根管中的 SL,同时具有最高的 EBS(10.13±0.69 MPa)。然而,第 1 组(5.25%次氯酸钠+17% EDTA)样本的根尖部(2.95±0.33)去除根管牙本质中的 SL 效果最差,氧化锆桩与牙本质之间的结合强度最低(5.11±0.19 MPa)。SYMPA 联合 17% EDTA 技术在去除根管牙本质中的 SL 并增强氧化锆桩的 EBS 方面非常有效。5.25%次氯酸钠+17% EDTA 是去除 SL 和提高 MH 最不理想的方法。CQDs 和 Nd: YAG 激光显示出从根管中去除 SL 的良好性能,同时达到了氧化锆桩适当的结合强度。研究亮点:Nd: YAG 激光和 17% EDTA 作为根管消毒剂具有最高的 MH 值。用 SYMPA 和 17% EDTA 冲洗的样本从根管中去除 SL 的效果最佳。第 3 组(SYMPA+17% EDTA)样本的冠部揭示了与根管牙本质结合的最高氧化锆桩完整性评分。不同实验组以黏合性失效为主。