Wang Dan, Ma Chao, Chen Ye, Gu Li, Yu Yangyang
Tianjin Renai College, Tianjin, 0086, CHN, China.
State Key Laboratory of Engines, Tianjin University, Tianjin, 0086, CHN, China.
Sci Rep. 2024 Apr 24;14(1):9468. doi: 10.1038/s41598-024-60309-x.
Microstructures and mechanical properties of Mg-12Gd-0.8Zn-0.4Zr (GZ1208K, wt.%) alloy under different treatments (as-cast: signed as nonHIP-GZ1208K, hot isostatic pressing (HIP): signed as HIP-GZ1208K) were characterized. Based on microstructure characterization, two prismatic precipitates, β' and β precipitates, and one basal precipitate, γ' precipitate, formed in both of nonHIP-GZ1208K and HIP-GZ1208K alloy. According to analysis, the area number density and the size of β' precipitate could be adjusted through HIP treatment. The area number density of β' precipitate increased after HIP treatment when aged at 32 h, and the size of β' precipitate refined in both of the HIP-GZ1208K alloy aged at 8 h and 32 h. Except the influence of HIP treatment on microstructures, the ultimate tensile strength (UTS) and elongation of nonHIP-GZ1208K alloy also improved after HIP treatment. The UTS of the GZ1208K alloy aged at 8 h increased from 348 MPa (nonHIP-) to 371 MPa (HIP-) and the elongation increased from 2.6% to 4.7%. The density of the nonHIP-GZ1208K alloy increased after HIP treatment, that is to say the casting defects could be eliminated and the compactness of microstructures could be increased under the high pressure of HIP treatment.
对Mg-12Gd-0.8Zn-0.4Zr(GZ1208K,重量百分比)合金在不同处理条件下(铸态:标记为nonHIP-GZ1208K,热等静压(HIP):标记为HIP-GZ1208K)的微观结构和力学性能进行了表征。基于微观结构表征,在nonHIP-GZ1208K和HIP-GZ1208K合金中均形成了两种棱柱形析出相,即β'和β析出相,以及一种基面析出相,即γ'析出相。分析表明,通过HIP处理可以调整β'析出相的面积数密度和尺寸。在32小时时效时,HIP处理后β'析出相的面积数密度增加,并且在8小时和32小时时效的HIP-GZ1208K合金中β'析出相的尺寸均得到细化。除了HIP处理对微观结构的影响外,HIP处理后nonHIP-GZ1208K合金的极限抗拉强度(UTS)和伸长率也有所提高。在8小时时效的GZ1208K合金中,UTS从348MPa(nonHIP-)增加到371MPa(HIP-),伸长率从2.6%增加到4.7%。HIP处理后nonHIP-GZ1208K合金的密度增加,也就是说,在HIP处理的高压下可以消除铸造缺陷并提高微观结构的致密性。