BaiLie School of Petroleum Engineering, Lanzhou City University, Lanzhou, China.
The NO.6 Oil Production Plant, PetroChina Changqing Oilfield Company, Dingbian, China.
PLoS One. 2024 Apr 26;19(4):e0298672. doi: 10.1371/journal.pone.0298672. eCollection 2024.
Aqueous phase trapping (APT), which is one of the most prominent damages, seriously restricts the natural gas production in tight gas sandstone with low permeability. Pore size and microscopic pore structures are the most important factors to determine the water blocking damage. In this paper, 9 core samples from tight gas sandstone with various physical properties were employed, and the pore size distribution (PSD) of the core samples were investigated by high pressure mercury intrusion tests (HPMI). Results showed that the porosity of core samples ranges from 5.68% to 13.7%, and the permeability ranges from 0.00456 to 7.86 mD, which is a typical tight reservoir with strong heterogeneity. According to the HPMI capillary curve, the cores can be divided into two types: Type I and Type II, and the pore sizes of type I are larger than that of type II. Fractal distributions were obtained using HPMI data to further determine the pore structure characteristics of tight reservoirs. The pore structures of tight sandstones display the multifractal fractal feature: D1 corresponding to macro-pores, and D2 corresponding to fractal dimension of micro-pores. Furthermore, APT damage was determined by the permeability recovery ratios (Kr) after gas flooding tests. The correlation of Kr and PSD and fractal dimensions were jointly analyzed in tight gas sandstone. Although positive correlations between pore size parameters and the permeability recovery ratios were observed with relatively weak correlations, for those core samples with very close permeability, pore size parameters (both permeability and PSD) is inadequate in clarifying this damage. The fractal dimension can well describe the complexity and heterogeneity of flow channels in pores, which can become the determining factor to distinguish the flow capacity of tight sandstone. The D2 for samples of type I and type II exhibited a good negative relation with Kr with a correlation coefficient of 0.9878 and 0.7723, respectively. The significance of this finding is that for tight gas sandstone, fractal dimensions, especially the small pore fractal dimension (D2), can be used to predict the possible APT damage very well.
水相圈闭(APT)是一种最突出的损害,严重限制了低渗透致密砂岩气的天然气产量。孔径和微观孔隙结构是决定水锁损害的最重要因素。本文采用 9 块具有不同物理性质的致密砂岩岩心样品,采用高压压汞试验(HPMI)研究岩心样品的孔径分布(PSD)。结果表明,岩心样品的孔隙度为 5.68%13.7%,渗透率为 0.004567.86mD,属于强非均质性致密储层。根据 HPMI 毛细曲线,将岩心分为两类:I 型和 II 型,I 型的孔径大于 II 型。利用 HPMI 数据得到分形分布,进一步确定致密储层的孔隙结构特征。致密砂岩的孔隙结构呈现多重分形分形特征:D1 对应于大孔,D2 对应于微孔的分形维数。此外,通过气体驱替试验后的渗透率恢复率(Kr)来确定 APT 损伤。在致密砂岩气中,共同分析 Kr 与 PSD 和分形维数的相关性。尽管观察到孔径参数与渗透率恢复率之间存在正相关关系,但相关性较弱,对于那些渗透率非常接近的岩心样品,孔径参数(渗透率和 PSD)不足以说明这种损害。分形维数可以很好地描述孔隙中流道的复杂性和非均质性,可以成为区分致密砂岩流动能力的决定因素。I 型和 II 型样品的 D2 与 Kr 呈良好的负相关关系,相关系数分别为 0.9878 和 0.7723。这一发现的意义在于,对于致密砂岩气,分形维数,特别是小孔分形维数(D2),可以很好地预测可能的 APT 损伤。