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基于明胶的含牛至精油/β-环糊精微胶囊控释抗菌膜的合成与应用,用于草鱼鱼片的冷藏保鲜。

Synthesis and application of gelatin-based controlled-release antibacterial films containing oregano essential oil/β-cyclodextrin microcapsules for chilling preservation of grass carp fillets.

机构信息

College of Food Science and Technology, Huazhong Agricultural University, Wuhan 430070, China.

College of Food Science and Technology, Huazhong Agricultural University, Wuhan 430070, China; National R & D Branch Center for Conventional Freshwater Fish Processing, Wuhan 430070, China.

出版信息

Food Chem. 2024 Sep 1;451:139465. doi: 10.1016/j.foodchem.2024.139465. Epub 2024 Apr 24.

Abstract

This work aimed to synthesize oregano essential oil/β-cyclodextrin microcapsules (OEO/β-CDs) and then prepare gelatin-based controlled-release antibacterial films with different OEO/β-CDs contents (0%-2%) for chilling preservation of grass carp fillets. The results of FTIR, XRD, DSC and accelerated release ratio showed that OEO was successfully encapsulated in OEO/β-CDs and its thermal stability was effectively improved. Moreover, at 2% of addition amount of OEO/β-CDs, the tensile strength of the films increased from 14.43 MPa to 18.72 MPa. In addition, the films showed significant antibacterial activity against Pseudomonas (61.52%), Aeromonas (62.87%), and Shewanella putrefaciens (66.67%). Preservation experiments showed that the films effectively prevented the increase of TVB-N, and TBA value of the refrigerated fillets and significantly suppressed the growth of spoilage organisms, thus extending the shelf life by 2-3 days. Therefore, the synthesized film has promising potential as an active packaging material for the preservation of grass carp.

摘要

本工作旨在合成牛至精油/β-环糊精微胶囊(OEO/β-CDs),然后制备不同 OEO/β-CDs 含量(0%-2%)的基于明胶的控释抗菌膜,用于冷藏草鱼片的保鲜。FTIR、XRD、DSC 和加速释放率的结果表明,OEO 成功地包埋在 OEO/β-CDs 中,其热稳定性得到有效提高。此外,当添加量为 2%的 OEO/β-CDs 时,膜的拉伸强度从 14.43 MPa 增加到 18.72 MPa。此外,该膜对假单胞菌(61.52%)、气单胞菌(62.87%)和腐败希瓦氏菌(66.67%)具有显著的抗菌活性。保鲜实验表明,该膜有效阻止了冷藏鱼片 TVB-N 和 TBA 值的增加,并显著抑制了腐败微生物的生长,从而将保质期延长了 2-3 天。因此,合成膜具有作为草鱼片保鲜的活性包装材料的广阔前景。

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