College of Food Science and Technology, Huazhong Agricultural University, Wuhan 430070, China.
College of Food Science and Technology, Huazhong Agricultural University, Wuhan 430070, China; National R & D Branch Center for Conventional Freshwater Fish Processing, Wuhan 430070, China.
Food Chem. 2024 Sep 1;451:139465. doi: 10.1016/j.foodchem.2024.139465. Epub 2024 Apr 24.
This work aimed to synthesize oregano essential oil/β-cyclodextrin microcapsules (OEO/β-CDs) and then prepare gelatin-based controlled-release antibacterial films with different OEO/β-CDs contents (0%-2%) for chilling preservation of grass carp fillets. The results of FTIR, XRD, DSC and accelerated release ratio showed that OEO was successfully encapsulated in OEO/β-CDs and its thermal stability was effectively improved. Moreover, at 2% of addition amount of OEO/β-CDs, the tensile strength of the films increased from 14.43 MPa to 18.72 MPa. In addition, the films showed significant antibacterial activity against Pseudomonas (61.52%), Aeromonas (62.87%), and Shewanella putrefaciens (66.67%). Preservation experiments showed that the films effectively prevented the increase of TVB-N, and TBA value of the refrigerated fillets and significantly suppressed the growth of spoilage organisms, thus extending the shelf life by 2-3 days. Therefore, the synthesized film has promising potential as an active packaging material for the preservation of grass carp.
本工作旨在合成牛至精油/β-环糊精微胶囊(OEO/β-CDs),然后制备不同 OEO/β-CDs 含量(0%-2%)的基于明胶的控释抗菌膜,用于冷藏草鱼片的保鲜。FTIR、XRD、DSC 和加速释放率的结果表明,OEO 成功地包埋在 OEO/β-CDs 中,其热稳定性得到有效提高。此外,当添加量为 2%的 OEO/β-CDs 时,膜的拉伸强度从 14.43 MPa 增加到 18.72 MPa。此外,该膜对假单胞菌(61.52%)、气单胞菌(62.87%)和腐败希瓦氏菌(66.67%)具有显著的抗菌活性。保鲜实验表明,该膜有效阻止了冷藏鱼片 TVB-N 和 TBA 值的增加,并显著抑制了腐败微生物的生长,从而将保质期延长了 2-3 天。因此,合成膜具有作为草鱼片保鲜的活性包装材料的广阔前景。