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激光烧结和注塑成型制备的玻璃微珠填充聚酰胺12试样的力学行为差异研究

On the Difference in Mechanical Behavior of Glass Bead-Filled Polyamide 12 Specimens Produced by Laser Sintering and Injection Molding.

作者信息

De Coninck Hellen, Meyers Sebastian, Van Puyvelde Peter, Van Hooreweder Brecht

机构信息

KU Leuven, Department of Mechanical Engineering, Manufacturing Processes and Systems (MaPS), Leuven, Belgium.

KU Leuven, Department of Chemical Engineering, Soft Matter, Rheology and Technology (SMaRT), Leuven, Belgium.

出版信息

3D Print Addit Manuf. 2024 Apr 1;11(2):419-433. doi: 10.1089/3dp.2022.0160. Epub 2024 Apr 16.

Abstract

An increasing demand for additively manufactured polymer composites with optimized mechanical properties is manifesting in different industries such as aerospace, biomedical, and automotive. Laser sintering (LS) is an additive manufacturing method that has the potential to produce reinforced polymers, which can meet the stringent requirements of these industries. For the development of a commercially viable LS nylon-based composite material, previous research studies worldwide have focused on adding glass beads to the powder material with the goal to produce fully dense parts with properties more representative of injection molded (IM) thermoplastic composites. This led to the development of a commercially available glass bead-filled polyamide 12 (PA12) powder. Although this powder has been on the market for quite a while, an in-depth comparison of the mechanical behavior of laser sintered versus IM glass bead-filled PA12 is lacking. In this study, laser-sintered glass bead-filled PA12 samples were built in different orientations and compared to IM counterparts. After sample production, the mechanical performance of the produced LS and IM parts was tested and compared to evaluate the quasistatic and dynamic mechanical performance and failure mechanisms at different load levels. In addition, the glass bead-filled PA12 properties were also compared to those of standard (unfilled) LS PA12 to assess whether glass beads actually improve the mechanical performance and fatigue lifetime of the final LS samples, as suggested in literature. Results in this work present and explain the increased stiffness but decreased fatigue life of glass bead-filled polyamide parts made by LS and IM. This research can be regarded as a "benchmark" study, in which samples produced from commercially available, filled and unfilled, PA12 powder grades are compared for both LS and conventional production techniques.

摘要

航空航天、生物医学和汽车等不同行业对具有优化机械性能的增材制造聚合物复合材料的需求日益增长。激光烧结(LS)是一种增材制造方法,有潜力生产增强聚合物,能够满足这些行业的严格要求。为了开发具有商业可行性的基于LS尼龙的复合材料,全球先前的研究主要集中在向粉末材料中添加玻璃珠,目标是生产出具有更能代表注塑(IM)热塑性复合材料性能的全致密零件。这促成了一种市售的玻璃珠填充聚酰胺12(PA12)粉末的开发。尽管这种粉末已在市场上销售了相当一段时间,但缺乏对激光烧结与注塑玻璃珠填充PA12的力学行为的深入比较。在本研究中,以不同取向制造了激光烧结玻璃珠填充PA12样品,并与注塑对应物进行比较。在样品生产后,对所生产的LS和IM零件的力学性能进行测试和比较,以评估不同载荷水平下的准静态和动态力学性能以及失效机制。此外,还将玻璃珠填充PA12的性能与标准(未填充)LS PA12的性能进行比较,以评估玻璃珠是否真如文献中所表明的那样提高了最终LS样品的力学性能和疲劳寿命。本研究结果展示并解释了通过LS和IM制造的玻璃珠填充聚酰胺零件刚度增加但疲劳寿命降低的现象。这项研究可被视为一项“基准”研究,其中对市售的填充和未填充PA12粉末等级通过LS和传统生产技术制造的样品进行了比较。

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