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介质阻挡放电(DBD)等离子体处理对小麦淀粉理化性能及 3D 打印性能的影响。

Effect of dielectric barrier discharge (DBD) plasma treatment on physicochemical and 3D printing properties of wheat starch.

机构信息

Shaanxi Union Research Center of University and Enterprise for Grain Processing Technologies, College of Food Science and Engineering, Northwest A & F University, Yangling 712100, China.

Graduate School of Bioagricultural Sciences, Nagoya University, Furo-Cho, Chikusa, Nagoya 464-8601, Japan.

出版信息

Int J Biol Macromol. 2024 Jun;269(Pt 2):132159. doi: 10.1016/j.ijbiomac.2024.132159. Epub 2024 May 7.

Abstract

In recent years, the focus has shifted towards carbohydrate-based hydrogels and their eco-friendly preparation methods. This study involved an investigation into the treatment of wheat starch using dielectric barrier discharge (DBD) plasma technology over varying time gradients (0, 2, 5, 10, 15, and 20 min). The objective was to systematically examine the impact of different treatment durations on the physicochemical properties of wheat starch and the suitability of its gels for 3D printing. Morphology of wheat starch remained intact after DBD treatment. However, it led to a reduction in the amylose content, molecular weight, and crystallinity. This subsequently resulted in a decrease in the pasting temperature and viscosity. Moreover, the gels of the DBD-treated starch exhibited superior 3D printing performance. After a 2-min DBD treatment, the 3D printed samples of the wheat starch gel showed no significant improvements, as broken bars were evident on the surface of the 3D printed graphic, whereas DBD-20 showed better printing accuracy and surface structure, compared to the original starch without slumping. These results suggested that DBD technology holds potential for developing new starch-based gels with impressive 3D printing properties.

摘要

近年来,人们的研究重点转向了基于碳水化合物的水凝胶及其环保型制备方法。本研究采用介质阻挡放电(DBD)等离子体技术,在不同的时间梯度(0、2、5、10、15 和 20 分钟)下处理小麦淀粉,探讨了其处理方法。目的是系统地研究不同处理时间对小麦淀粉理化性质的影响,以及其凝胶在 3D 打印中的适用性。DBD 处理后,小麦淀粉的形态保持完整,但直链淀粉含量、分子量和结晶度降低,糊化温度和黏度也随之降低。此外,DBD 处理后的淀粉凝胶具有更好的 3D 打印性能。经过 2 分钟的 DBD 处理,小麦淀粉凝胶的 3D 打印样品并没有显著改善,因为在 3D 打印图形的表面可以明显看到断裂的棒状结构,而 DBD-20 与未膨化的原始淀粉相比,具有更好的打印精度和表面结构。这些结果表明,DBD 技术在开发具有优异 3D 打印性能的新型淀粉基凝胶方面具有潜力。

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