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氧化锌对铽激活硼硅酸锌玻璃发光性能的影响

Effect of ZnO on Luminescence Performance of Terbium-Activated Zinc Borosilicate Glasses.

作者信息

Dayioglugil Sena, Solak Nuri

机构信息

Faculty of Chemical-Metallurgical Engineering, Istanbul Technical University, Istanbul 34469, Turkey.

出版信息

Materials (Basel). 2024 May 4;17(9):2154. doi: 10.3390/ma17092154.

DOI:10.3390/ma17092154
PMID:38730960
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC11084722/
Abstract

In this study, terbium-doped ZnO-SiO-BO-NaO glasses were fabricated with the conventional melt-quenching method. The effect of altering the concentration of the host matrix on luminescence performance was investigated in terms of different ZnO/BO and ZnO/SiO ratios. FT-IR results indicate that bridging oxygens (Bos) were converted to non-bridging oxygens (NBOs) with increments of ZnO. Furthermore, the emission intensity and luminescence lifetime of samples were influenced by the amount of ZnO; this was proven with photoluminescence spectra results. The maximum emission intensity was observed at a 1.1 ZnO/BO ratio and a 0.8 ZnO/SiO ratio; however, the highest luminescence lifetime was observed at a 1.1 ZnO/SiO ratio. The emission intensity and luminescence lifetime of glass samples were improved by heat treatment as a result of the formation of willemite and zinc oxide phases. An increase in the ZnO/SiO ratio facilitated the formation of willemite and zinc oxide phases; therefore, crystallinity was directly related to the luminescence behavior of glass samples.

摘要

在本研究中，采用传统的熔体淬火法制备了掺铽的ZnO-SiO-BO-NaO玻璃。通过不同的ZnO/BO和ZnO/SiO比率，研究了改变主体基质浓度对发光性能的影响。傅里叶变换红外光谱（FT-IR）结果表明，随着ZnO含量的增加，桥氧（Bos）转变为非桥氧（NBOs）。此外，样品的发射强度和发光寿命受ZnO含量的影响；光致发光光谱结果证实了这一点。在ZnO/BO比率为1.1和ZnO/SiO比率为0.8时观察到最大发射强度；然而，在ZnO/SiO比率为1.1时观察到最高发光寿命。由于硅锌矿和氧化锌相的形成，玻璃样品的发射强度和发光寿命通过热处理得到改善。ZnO/SiO比率的增加促进了硅锌矿和氧化锌相的形成；因此，结晶度与玻璃样品的发光行为直接相关。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c870/11084722/d875a1bc49ab/materials-17-02154-g012.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c870/11084722/01d43ff2fa6d/materials-17-02154-g009.jpg
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J Inorg Organomet Polym Mater. 2022;32(3):941-953. doi: 10.1007/s10904-021-02183-y. Epub 2022 Jan 18.