Materials, Membranes and Nanotechnology Laboratory, Faculty of Sciences, University of Moulay Ismail, P. O. Box 11201, Zitoune, Meknes 50060, Morocco.
Faculty of Sciences, Laboratory of Biotechnologies and Valorisation of Bioresources, Moulay Ismaïl University of Meknes, BP 11201, Zitoune, Meknes, Morocco; Cluster of Competencies Agri-food and Food Safety, Moulay Ismail University of Meknes, Marjane 2, BP 298, Meknes, Morocco.
Water Sci Technol. 2024 Jun;89(11):2921-2935. doi: 10.2166/wst.2024.175. Epub 2024 May 28.
This paper centers on the preparation and characterization of both a clay support and a faujasite zeolite membrane. Additionally, the study explores the development of bacterial media to assess the performance of these prepared membranes. The faujasite zeolite membrane was created using the hydrothermal method, involving the deposition of a faujasite layer to fine-tune the pore sizes of the clay support. The clay supports were crafted from clay which was sieved to particle size Φ ≤ 63 μm, and compacted with 3.0 wt.% activated carbon, then sintered at 1,000 °C. Distilled water fluxes revealed a decrease from 1,500 L m h to a minimum of 412 L m h after 180 min of filtration. Both membranes were characterized by XRF, XRD, FTIR, adsorption-desorption of nitrogen (N), and SEM-EDS. PCR technique was used for the identification of the isolated sp., and the retention of the bacteria on the clay support and the faujasite zeolite membrane were found to be 96 and 99%, respectively. The results showed that the faujasite zeolite membrane passed the clay support due to a narrow pore size of the faujasite zeolite membrane of 2.28 nm compared to 3.55 nm for the clay supports.
本文主要研究了粘土载体和丝光沸石膜的制备与表征。此外,还研究了细菌培养基的开发,以评估这些制备的膜的性能。丝光沸石膜是采用水热法制备的,包括沉积丝光沸石层以微调粘土载体的孔径。粘土载体由筛分到粒径 Φ ≤ 63 μm 的粘土制成,并用 3.0wt.%的活性炭压实,然后在 1000°C下烧结。过滤 180 分钟后,水通量从 1500 L m h 降至最低 412 L m h。两种膜均通过 XRF、XRD、FTIR、氮(N)吸附-解吸和 SEM-EDS 进行了表征。采用 PCR 技术鉴定了分离出的 sp.,发现细菌在粘土载体和丝光沸石膜上的保留率分别为 96%和 99%。结果表明,由于丝光沸石膜的孔径为 2.28nm,而粘土载体的孔径为 3.55nm,因此丝光沸石膜通过了粘土载体。