Li Zhihua, Wang Siwen, Qin Zhou, Fang Wenbing, Guo Ziang, Zou Xiaobo
School of Food and Biological Engineering, Jiangsu University, Zhenjiang 212013, China.
Gels. 2024 Jun 27;10(7):425. doi: 10.3390/gels10070425.
The objective of this study was to develop a food 3D printing gel and investigate the effects of whey protein isolate (WPI), sodium alginate (SA), and water-bath heating time on the 3D printing performance of the gel. Initially, the influence of these three factors on the rheological properties of the gel was examined to determine the suitable formulation ranges for 3D printing. Subsequently, the formulation was optimized using response surface methodology, and texture analysis, scanning electron microscopy (SEM), and Fourier-transform infrared (FTIR) spectroscopy were conducted. The rheological results indicated that gels with WPI concentrations of 6-7 g, SA concentrations of 0.8-1.2 g, and water-bath heating times of 10-12 min exhibited lower yield stress and better self-supporting properties. The optimized formulation, determined through response surface methodology, consisted of 1.2 g SA, 6.5 g WPI, and a heating time of 12 min. This optimized formulation demonstrated enhanced extrusion capability and superior printing performance. SEM analysis revealed that the optimized gel possessed good mechanical strength, and FTIR spectroscopy confirmed the successful composite formation of the gel. Overall, the results indicate that the optimized gel formulation can be successfully printed and exhibits excellent 3D printing performance.
本研究的目的是开发一种食品3D打印凝胶,并研究乳清蛋白分离物(WPI)、海藻酸钠(SA)和水浴加热时间对该凝胶3D打印性能的影响。首先,考察这三个因素对凝胶流变学性质的影响,以确定适合3D打印的配方范围。随后,采用响应面法对配方进行优化,并进行了质地分析、扫描电子显微镜(SEM)和傅里叶变换红外(FTIR)光谱分析。流变学结果表明,WPI浓度为6 - 7 g、SA浓度为0.8 - 1.2 g、水浴加热时间为10 - 12 min的凝胶表现出较低的屈服应力和较好的自支撑性能。通过响应面法确定的优化配方为1.2 g SA、6.5 g WPI和加热时间12 min。这种优化配方表现出增强的挤出能力和优异的打印性能。SEM分析表明优化后的凝胶具有良好的机械强度,FTIR光谱证实了凝胶的成功复合形成。总体而言,结果表明优化后的凝胶配方能够成功打印并表现出优异的3D打印性能。