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增材制造氧化锆修复体的机械性能和冠精度。

Mechanical properties and crown accuracy of additively manufactured zirconia restorations.

机构信息

Department of Prosthodontics, College of Dentistry, Yonsei University, Seoul 03722, Republic of Korea.

Department of Prosthodontics and Dental Research Institute, Seoul National University School of Dentistry, 101 Daehak-ro, Jongno-gu, Seoul 03080, Republic of Korea.

出版信息

Dent Mater. 2024 Oct;40(10):1546-1556. doi: 10.1016/j.dental.2024.07.016. Epub 2024 Jul 26.

Abstract

OBJECTIVES

We evaluated the mechanical properties of zirconia restorations produced via additive manufacturing (AM) and the crown accuracy of zirconia crowns.

METHODS

Zirconia disks, bars, and crowns were manufactured via subtractive (CNC group) and additive manufacturing (AM group) techniques. Disk-shaped specimens in each group were autoclaved at 134 °C and 216 kPa for 5, 10, and 24 h. The phases of the specimens were analyzed using an X-ray diffractometer. The flexural strengths were measured via biaxial flexural tests. The morphologies were examined using a scanning electron microscope. The correlation between the m-phase fraction and biaxial flexural strength by autoclave time in each group was analyzed via linear mixed model and Pearson's correlation analysis. For each group, crown specimens were used to assess the marginal and internal gaps using the replica technique. Buccolingual and mesiodistal cross-sections were measured, and a repeated measures one-way ANOVA was performed.

RESULTS

Linear mixed model analysis indicated that for both groups, with an increase in the autoclave time, the flexural strength decreased, whereas the m-phase fraction increased. Pearson's correlation analysis revealed no correlation between the m-phase fraction and flexural strength for either group. A repeated measures one-way ANOVA was conducted on instrumented sections (buccal, lingual, mesial, and distal), revealing that the marginal and internal gaps of AM-produced zirconia crowns were less accurate than those of CNC-produced zirconia crowns.

SIGNIFICANCE

These findings suggest that additively produced zirconia restorations have mechanical properties comparable to those of conventionally produced ceramics and may be suitable for clinical applications.

摘要

目的

评估通过增材制造(AM)生产的氧化锆修复体的机械性能和氧化锆冠的冠精度。

方法

通过减法(CNC 组)和加法制造(AM 组)技术制造氧化锆圆盘、棒材和冠。每组中的盘形试件在 134°C 和 216 kPa 下分别进行 5、10 和 24 h 的高压蒸汽灭菌。使用 X 射线衍射仪分析试件的相。通过双向弯曲试验测量弯曲强度。使用扫描电子显微镜检查形貌。通过线性混合模型和 Pearson 相关分析分析每组中 m 相分数与高压蒸汽灭菌时间的双轴弯曲强度之间的相关性。对于每组,使用复制技术评估冠试件的边缘和内部间隙。测量颊舌和近远中截面,并进行重复测量单向方差分析。

结果

线性混合模型分析表明,对于两组,随着高压蒸汽灭菌时间的增加,弯曲强度降低,而 m 相分数增加。Pearson 相关分析表明,两组的 m 相分数与弯曲强度之间均无相关性。对仪器化部分(颊侧、舌侧、近中侧和远中侧)进行重复测量单向方差分析,结果表明,AM 生产的氧化锆冠的边缘和内部间隙不如 CNC 生产的氧化锆冠精确。

意义

这些发现表明,通过增材制造生产的氧化锆修复体具有与传统生产的陶瓷相当的机械性能,可能适用于临床应用。

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