Kassas Ahmad, Zahwa Israa, Hussein Bassam, Bernard Jérôme, Lelièvre Céline, Mouyane Mohamed, Noudem Jacques, Houivet David
The International University of Beirut, School of Engineering, Department of Industrial Engineering, Beirut, Lebanon.
LUSAC-EA4253, Université de Caen Basse-Normandie, Rue Louis Aragon, BP 78, 50130, CHERBOURG-OCTEVILLE, France.
Heliyon. 2024 Jul 2;10(13):e33999. doi: 10.1016/j.heliyon.2024.e33999. eCollection 2024 Jul 15.
The fabrication of low-porosity ceramics for humidity sensing is crucial to prevent moisture entrapment, which poses significant challenges. Using Spark Plasma Sintering (SPS), we successfully densified fine-grained ceramic materials based on LiF-doped MgTiO, comparing them with conventionally sintered counterparts. Structural and microstructural analyses, employing X-ray diffraction and Scanning Electron Microscopy (SEM), were conducted. Investigation into electrical and dielectric properties' variations concerning humidity levels was conducted and revealed that SPS sintered ceramics exhibit heightened sensitivity to moisture, as evidenced by resistivity, capacitance, and response time measurements. The implications of these results are discussed in depth, highlighting the potential of SPS as a promising method for fabricating humidity sensors with improved performance and reduced porosity-related issues.
制造用于湿度传感的低孔隙率陶瓷对于防止水分截留至关重要,而这带来了重大挑战。我们使用放电等离子烧结(SPS)成功地将基于掺LiF的MgTiO的细晶粒陶瓷材料致密化,并将其与传统烧结的对应材料进行比较。采用X射线衍射和扫描电子显微镜(SEM)进行了结构和微观结构分析。对湿度水平相关的电学和介电性能变化进行了研究,结果表明,通过电阻率、电容和响应时间测量证明,SPS烧结陶瓷对湿度表现出更高的灵敏度。深入讨论了这些结果的意义,突出了SPS作为一种有前景的方法在制造性能改进且孔隙率相关问题减少的湿度传感器方面的潜力。