Department of Prosthodontics, Seoul St. Mary's Dental Hospital, College of Medicine, The Catholic University of Korea, Banpo-daero 222, Seocho-gu, Seoul, 06591, Republic of Korea.
Department of Cariology and Operative Dentistry, Graduate School of Medical and Dental Sciences, Tokyo Medical and Dental University (TMDU), 1-5-45, Yushima, Bunkyo-ku, Tokyo, 113-8549, Japan.
Clin Oral Investig. 2024 Aug 2;28(8):463. doi: 10.1007/s00784-024-05858-1.
The first aim of this study was to determine whether there is a difference in degree of conversion (DC) of touch-cure cements polymerized by self-curing with adhesive or dual-curing under reduced light. The second aim was to compare interfacial adaptation of zirconia restoration cemented using touch-cure cements self-cured or dual-cured by reduced light.
The DC of touch-cure resin cements with adhesive was measured continuously using Fourier transform infrared spectrometry. Experimental groups differed depending on touch-cure cement. Each group had three subgroups of polymerization method. For subgroup 1, the DC was measured by self-curing. For subgroups 2 and 3, the DCs were measured by dual-curing with reduced light penetrating 3 mm and 1 mm zirconia blocks, respectively. For interfacial adaptation evaluation, Class I cavity was prepared on an extracted third molar, and zirconia restoration was fabricated. The restoration was cemented using the same cement. Groups and subgroups for interfacial adaptation were the same as those of the DC measurement. After thermo-cycling, interfacial adaptation at the tooth-restoration interface was evaluated using swept-source optical coherence tomography imaging.
The DC of touch-cure cement differed depending on the measurement time, resin cement, and polymerization method (p < 0.05). Interfacial adaptation was different depending on the resin cement and polymerization method (p < 0.05).
For touch-cure cement, light-curing with higher irradiance presented a higher DC and superior interfacial adaptation than light-curing with lower irradiance or self-curing.
Although some adhesives accelerate the self-curing of touch-cure cement, light-curing for touch-cure cement is necessary for zirconia cementation.
本研究的首要目的是确定自固化与黏接辅助光固化、低强度光固化两种方式对触变性树脂水门汀聚合转化率(DC)的影响是否存在差异。其次,比较黏接辅助光固化与低强度光固化两种方式对氧化锆修复体粘接效果的影响。
采用傅里叶变换红外光谱法连续测量触变性树脂水门汀的 DC。根据触变性树脂水门汀的不同,将实验分为若干组。每组根据聚合方式的不同,又分为 3 个亚组。亚组 1 采用自固化,亚组 2 和亚组 3 分别采用低强度光透过 3mm 和 1mm 氧化锆块的双固化。在第三磨牙上制备 I 类洞型,制作氧化锆修复体,采用相同的水门汀进行粘接。聚合方式与 DC 测量时的分组方式相同。热循环后,采用扫频源光学相干断层扫描评估牙体-修复体界面的结合情况。
触变性树脂水门汀的 DC 随测量时间、树脂水门汀种类和聚合方式的不同而变化(p<0.05)。树脂水门汀种类和聚合方式对界面适应性也有影响(p<0.05)。
对于触变性树脂水门汀,高光照强度的光固化比低光照强度或自固化具有更高的 DC 和更好的界面适应性。
尽管一些黏接剂可以加速触变性树脂水门汀的自固化,但对于氧化锆粘接,触变性树脂水门汀仍需要光固化。