Huang Chen, Tang Junjie, Chen Xingyan, Zeng Xinxin, Zhong Weiquan, Pang Jie, Wu Chunhua
College of Food Science, Fujian Agriculture and Forestry University, Fuzhou 350002, China.
Foods. 2024 Aug 14;13(16):2538. doi: 10.3390/foods13162538.
In this study, a series of novel nanofibers based on gelatin (GA) loading with purple potato anthocyanin (PPA) and syringic acid (SA) were obtained by electrospinning technology. The effects of SA on mechanical properties, thermal stability, antioxidant capacity, and antimicrobial activity of the GA/PPA nanofibers were systematically characterized. The scanning electron microscopy observation results revealed a smooth surface on the nanofibers. The incorporation of SA enhanced the viscosity of the electrospun solutions, and it increased the average diameter of nanofibers from 0.17 μm to 0.28 μm. The tensile strength and thermal stability of the obtained nanofibers were enhanced with the addition of a suitable level of SA (1.5%, /), which strengthened the intermolecular interaction. The GA/PPA/SA nanofibers presented over 80% antioxidant capacity and strong antibacterial activity against and . Meanwhile, the sensitivity responses of nanofibers to NH revealed that GA/PPA/SA II nanofibers (1.5% / SA) presented good sensitivity of colorimetric behavior to ammonia. A pork spoilage test was performed to evaluate practical application of the nanofibers, and an obvious color change (dark purple to green) was observed. These results indicated GA/PPA/SA II nanofibers can be utilized as an active and intelligent multipurpose packaging material to preserve and track the freshness of pork.
在本研究中,通过静电纺丝技术制备了一系列负载紫薯花青素(PPA)和丁香酸(SA)的新型明胶(GA)基纳米纤维。系统地表征了SA对GA/PPA纳米纤维的力学性能、热稳定性、抗氧化能力和抗菌活性的影响。扫描电子显微镜观察结果显示纳米纤维表面光滑。SA的加入提高了静电纺丝溶液的粘度,并使纳米纤维的平均直径从0.17μm增加到0.28μm。添加适量的SA(1.5%,/)可增强所得纳米纤维的拉伸强度和热稳定性,这加强了分子间相互作用。GA/PPA/SA纳米纤维表现出超过80%的抗氧化能力以及对[具体菌种1]和[具体菌种2]的强抗菌活性。同时,纳米纤维对NH的敏感响应表明,GA/PPA/SA II纳米纤维(1.5% / SA)对氨呈现出良好的比色行为敏感性。进行了猪肉腐败试验以评估纳米纤维的实际应用,观察到明显的颜色变化(从深紫色变为绿色)。这些结果表明,GA/PPA/SA II纳米纤维可作为一种活性和智能的多功能包装材料,用于保存和追踪猪肉的新鲜度。