Annanya Arora, Ramadoss Ramya, Sundar Sandhya, Panneer Selvam Suganya, K Hemashree
Oral Pathology and Oral Biology, Saveetha Institute of Medical and Technical Sciences, Chennai, IND.
Cureus. 2024 Jul 29;16(7):e65696. doi: 10.7759/cureus.65696. eCollection 2024 Jul.
Introduction X-rays and X-ray diffraction (XRD) are two non-destructive techniques that determine a material's crystallographic structure, chemical composition, and physical properties. They can also be used to estimate a person's age when it is unknown, assess the need for orthodontic treatment, or predict the likelihood of tooth decay. This research aims to validate the accuracy of age estimation through X-ray diffraction analysis of tooth hard tissue with compositional changes. Methodology Four tooth samples were analyzed using the Pan Analytical XRD (Malvern Panalytical Ltd., UK) unique d8 family platform, which uses Cu Kα radiation (0.154 nm) and a 0.02° scan rate from 0 to 80°. Results The angle of incidence (ω) is established between the sample and the X-ray source. The angle of diffraction, 2θ, is established between the detector and the incident beam. The detector angle 2θ and the incident angle ω always equal half. Inter-atomic distance, or d-spacing (D = 10^-8 cm in Angstrom units), is measured. A greater crystal size or a greater degree of crystallinity may be indicated by a higher peak intensity, which translates to an increased amount of atoms in the crystal. Conclusion The study's findings suggest that XRD is a promising new technique for age determination, as it has an advanced and dynamic approach to finding the crystallographic characteristics of the provided sample.
引言
X射线和X射线衍射(XRD)是两种无损技术,可用于确定材料的晶体结构、化学成分和物理性质。当一个人的年龄未知时,它们还可用于估计其年龄、评估正畸治疗的必要性或预测龋齿的可能性。本研究旨在通过对具有成分变化的牙齿硬组织进行X射线衍射分析来验证年龄估计的准确性。
方法
使用帕纳科分析型X射线衍射仪(英国马尔文帕纳科有限公司)独特的d8系列平台对四个牙齿样本进行分析,该平台使用铜Kα辐射(0.154纳米),扫描速率为0.02°,扫描范围为0至80°。
结果
确定样品与X射线源之间的入射角(ω)。确定探测器与入射光束之间的衍射角(2θ)。探测器角度2θ与入射角ω始终相等。测量原子间距离,即d间距(以埃为单位,D = 10^-8厘米)。更高的峰值强度可能表明晶体尺寸更大或结晶度更高,这意味着晶体中的原子数量增加。
结论
该研究结果表明,XRD是一种很有前景的年龄测定新技术,因为它采用先进且动态的方法来发现所提供样品的晶体学特征。