Crispim Anne Heloyse Teixeira, da Silva Sarah Emille Gomes, de Gois Moreira Fernanda Gurgel, da Silva Bianca Cristina Dantas, de Medeiros Paulo Joadi Guerra Lima, Souza Rodrigo Othávio de Assunção E
Department of Dentistry, Federal University of Rio Grande do Norte (UFRN), Av. Salgado Filho, 1787, Lagoa Nova, Natal, RN, CEP: 59056-000, Brazil.
Analytical Center Technician, Institute of Chemistry, Federal University of Rio Grande do Norte (UFRN), Av. Salgado Filho, 3000, Lagoa Nova, Natal, RN, CEP:59078-970, Brazil.
Odontology. 2025 Apr;113(2):619-633. doi: 10.1007/s10266-024-00991-5. Epub 2024 Sep 6.
To evaluate the effect of build direction, post-polymerization time, and aging on the fracture resistance, failure mode, margin quality and Marginal (MD) and Internal Discrepancies (ID), and degree of conversion of tridimensional (3D) printed provisional crowns using the liquid crystal display technique (LCD). A left mandibular first molar was prepared and scanned. After, a full crown was designed (ExoCad) and exported to the LCD-printer software. One hundred and eighty crowns were printed at two build directions (30°, 90°) and post-polymerized for different periods (15, 30, 45 min). Half of the samples were aged (ST) in distilled water (37 °C/90 days). The marginal quality of the crowns was evaluated by the Schriwer method under a stereomicroscope (40x). The replica technique was used to measure the MD and ID and measured under a stereomicroscope (10x), through 20 reference points defined in 5 regions: Occlusal (O), Cusp (CP), Axial (AX), Chamfer (CH), and Finish Line (F). After, the crowns were cemented onto the respective dies using temporary cement and submitted to compression test (ISO150, 1 mm/min, 100 kgf).The failure mode was classified by Burke's fracture mode. The degree of conversion was evaluated through Fourier Transform Infrared Spectroscopy. The data (μm) of MD and ID and fracture resistance (N) were subjected to ANOVA (3 factors) and Tukey's test (5%); Weibull analysis was also performed for fracture resistance data (N). For MD, ID and fracture resistance ANOVA revealed that all factors (P < .001) were significant. For aged groups, the crowns printed at 30° showed lower MD (Tukey). The O_90_30 min (172.13 μm) and O_90_15 min (170.20 μm) groups showed the highest ID values. Higher resistance values were observed for the 30_45 min (844.30 N), 30_30 min (835.35 N), and 90_30 min (820.62 N) groups (Tukey). In the margin analysis, 98.6% of the crowns printed at 30° showed smooth margins without defects. The most prevalent fracture mode (41.7%) was Burke type 5. The degree of conversion (DC) increased with increasing post-polymerization time and aging. Printing provisional crowns at 30° provided lower crown MD and ID, as well as higher fracture resistance. A post-polymerization time of 30 min resulted in higher crown fracture resistance, while aging reduced the resistance of the crowns.
为评估成型方向、聚合后时间和老化对使用液晶显示技术(LCD)3D打印临时冠的抗折性、失效模式、边缘质量、边缘(MD)和内部差异(ID)以及固化程度的影响。制备并扫描一颗左下颌第一磨牙。之后,设计一个全冠(ExoCad)并导出到LCD打印机软件。在两个成型方向(30°、90°)打印180个冠,并在不同时间段(15、30、45分钟)进行后聚合。一半的样品在蒸馏水(37°C/90天)中老化(ST)。在体视显微镜(40倍)下通过施里弗方法评估冠的边缘质量。使用复制技术测量MD和ID,并在体视显微镜(10倍)下通过在5个区域定义的20个参考点进行测量:咬合面(O)、牙尖(CP)、轴面(AX)、肩台(CH)和边缘线(F)。之后,使用临时粘结剂将冠粘结到各自的代型上,并进行压缩试验(ISO150,1mm/min,100kgf)。失效模式根据伯克的骨折模式分类。通过傅里叶变换红外光谱评估固化程度。MD和ID的数据(μm)以及抗折性(N)进行三因素方差分析(ANOVA)和Tukey检验(5%);还对抗折性数据(N)进行威布尔分析。对于MD、ID和抗折性,方差分析显示所有因素(P<0.001)均具有显著性。对于老化组,在30°打印的冠显示出较低的MD(Tukey检验)。O_90_30分钟(172.13μm)和O_90_15分钟(170.20μm)组显示出最高的ID值。在30_45分钟(844.30N)、30_30分钟(835.35N)和90_30分钟(820.62N)组中观察到较高的抗折值(Tukey检验)。在边缘分析中,98.6%在30°打印的冠显示边缘光滑无缺陷。最常见的骨折模式(41.7%)是伯克5型。固化程度(DC)随着聚合后时间和老化的增加而增加。在30°打印临时冠可提供较低的冠MD和ID,以及较高的抗折性。30分钟的聚合后时间导致较高的冠抗折性,而老化会降低冠的抗折性。