Pereira Anne Karoline de Holanda Cavalcanti, Costa Rayanna Thayse Florêncio, Leão Rafaella de Souza, Casado Bruno Gustavo da Silva, Batista Andre Ulisses Dantas, Moraes Sandra Lúcia Dantas
Department of Oral Rehabilitation, Faculty of Dentistry, University of Pernambuco (FOP/UPE), Recife, Brazil.
Department of Dentistry, Federal University of Paraíba (UFPB), João Pessoa, Paraíba, Brazil.
J Prosthodont. 2024 Sep 21. doi: 10.1111/jopr.13941.
To investigate the effects of different surface treatments and thermal cycling on the shear bond strength between 3D-printed teeth and denture bases.
For the shear bond strength (SBS) test, the specimens were the maxillary central incisors (11 × 9 × 7 mm) bonded on a cylindrical base (20 × 25 mm). The control group was heat-cured polymethylmethacrylate (PMMA) (N = 20). The printed group was divided into five subgroups (N = 20): no treatment, sandblasting with aluminum oxide (AlO), methyl methacrylate monomer, acetone, and adhesive with urethane dimethacrylate. Half of the samples were subjected to 2000 thermal cycling cycles, and all samples were subjected to the SBS test. The failure mode was established as adhesive, cohesive, or mixed through stereomicroscopic analysis. The surface roughness test (Sa) was performed using optical profilometry, and the rectangular specimens (14 × 14 × 2.5 mm) were divided into four groups according to the surface treatments (N = 7 per group). Paired T and Wilcoxon tests were conducted to perform comparisons within the same group. The Kruskal-Wallis and Dwass-Steel-Critchlow-Fligner post-hoc tests were conducted to compare the groups.
AlO sandblasting in the 3D-printed groups achieved high SBS values comparable to those of the control group in the thermal cycled (p = 0.962) and non-thermal cycled samples (p = 0.319). It was the only treatment capable of modifying the surface of the 3D-printed resin, thereby increasing the roughness (p = 0.016).
Sandblasting is recommended to increase the bond strength between the tooth and denture bases.
研究不同表面处理和热循环对3D打印牙齿与义齿基托之间剪切粘结强度的影响。
对于剪切粘结强度(SBS)测试,标本为粘结在圆柱形底座(20×25mm)上的上颌中切牙(11×9×7mm)。对照组为热固化聚甲基丙烯酸甲酯(PMMA)(N = 20)。打印组分为五个亚组(N = 20):未处理、用氧化铝(AlO)喷砂、甲基丙烯酸甲酯单体、丙酮以及含双甲基丙烯酸聚氨酯的粘合剂。一半样品进行2000次热循环,所有样品均进行SBS测试。通过体视显微镜分析确定失效模式为粘结、内聚或混合。使用光学轮廓仪进行表面粗糙度测试(Sa),并根据表面处理将矩形标本(14×14×2.5mm)分为四组(每组N = 7)。进行配对T检验和威尔科克森检验以在同一组内进行比较。进行克鲁斯卡尔 - 沃利斯检验和德瓦斯 - 斯蒂尔 - 克里奇洛 - 弗利格纳事后检验以比较各组。
3D打印组中的AlO喷砂在热循环(p = 0.962)和非热循环样品(p = 0.319)中均获得了与对照组相当的高SBS值。它是唯一能够改变3D打印树脂表面的处理方法,从而增加粗糙度(p = 0.016)。
建议进行喷砂处理以增加牙齿与义齿基托之间的粘结强度。