Department of Prosthodontics, Faculty of Dentistry, Gazi University, Bişkek Cad. 1.Sk. No:4 06490 Emek, Ankara, Turkey.
Odontology. 2023 Oct;111(4):953-970. doi: 10.1007/s10266-023-00806-z. Epub 2023 Apr 4.
The high cost of CAD/CAM systems and materials is a severe economic burden. Therefore, repair of CAD/CAM PMMA, selecting appropriate repair materials, and surface modifications are clinically important. This study aims to evaluate the shear bond strength of PMMA repair materials after various surface treatments on CAD/CAM PMMA denture base material. For this purpose, a total of 480 CAD/CAM PMMA denture base test specimens were manufactured. Then all test specimens were divided into 6 groups, and different surface treatments were applied. Group A: sandblasting, Group B: 4% hydro fluoric acid, Group C: tungsten carbide bur, Group D: dichloromethane + methyl methacrylate mixture, Group E: dichloromethane and methyl methacrylate, Group F: no surface treatment. Each group is then divided into 4 different subcategories; repair processes were performed using; heat-cured acrylic resin (n:20), auto-polymerized acrylic resin (n:20), gingiva composite (n:20), and CAD/CAM PMMA tooth material (n:20). After repairs, thermal aging was applied to half of the test specimens in each subcategory. The shear bond strength value was measured with a universal test device. Sandblasting group showed the highest surface roughness value in all test specimens (p < 0.001). Heat-cured acrylic resin with sandblasting exhibited the highest bond strength, while the untreated gingiva composite resin exhibited the lowest value. Thermal aging decreased bond strength in all repair materials (p < 0.001). Among the surface treatment groups, sandblasting with AlO particles exhibited the highest surface roughness value and repair bond strength. The application of organic solvents to the surface increased the surface roughness and repair bond strength. Applying dichloromethane and methyl methacrylate monomer separately is more effective than applying it as a mixture. The ideal bonding among repair materials was obtained with heat-cured acrylic resin.
CAD/CAM 系统和材料的高成本是一个严重的经济负担。因此,修复 CAD/CAM PMMA、选择合适的修复材料和表面改性在临床实践中非常重要。本研究旨在评估 CAD/CAM PMMA 义齿基托材料经过不同表面处理后 PMMA 修复材料的剪切结合强度。为此,共制作了 480 个 CAD/CAM PMMA 义齿基托测试样本。然后,将所有测试样本分为 6 组,并进行不同的表面处理。A 组:喷砂处理,B 组:4%氢氟酸,C 组:碳化钨车针,D 组:二氯甲烷+甲基丙烯酸甲酯混合物,E 组:二氯甲烷和甲基丙烯酸甲酯,F 组:无表面处理。每组又分为 4 个不同的亚组;分别采用热固性丙烯酸树脂(n:20)、自聚物丙烯酸树脂(n:20)、牙龈复合材料(n:20)和 CAD/CAM PMMA 牙材料(n:20)进行修复。修复后,将每个亚组的一半测试样本进行热老化处理。使用万能试验机测量剪切结合强度值。在所有测试样本中,喷砂组的表面粗糙度值最高(p<0.001)。经过喷砂处理的热固性丙烯酸树脂具有最高的结合强度,而未经处理的牙龈复合材料的结合强度最低。所有修复材料的热老化均降低了结合强度(p<0.001)。在表面处理组中,AlO 颗粒喷砂处理的表面粗糙度值和修复结合强度最高。将有机溶剂应用于表面会增加表面粗糙度和修复结合强度。单独应用二氯甲烷和甲基丙烯酸甲酯单体比将其作为混合物应用更有效。热固性丙烯酸树脂可实现修复材料之间的理想结合。