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一种获取单体戊二醛的快速方法。

A rapid method for obtaining monomeric glutaraldehyde.

作者信息

Dijk F, Oosterbaan J A, Hulstaert C E

出版信息

Histochemistry. 1985;83(6):573-4. doi: 10.1007/BF00492463.

DOI:10.1007/BF00492463
PMID:3936824
Abstract

A new method for the distillation of glutaraldehyde to obtain the monomeric form is presented. The monomer is obtained after only one distillation and it has a purification index (Pi) smaller than 0.20.

摘要

提出了一种蒸馏戊二醛以获得单体形式的新方法。仅经过一次蒸馏即可获得单体，其纯化指数（Pi）小于0.20。

相似文献

1
A rapid method for obtaining monomeric glutaraldehyde.一种获取单体戊二醛的快速方法。
Histochemistry. 1985;83(6):573-4. doi: 10.1007/BF00492463.
2
[Method of purifying glutaraldehyde for microscopic research on biological objects].[用于生物物体微观研究的戊二醛纯化方法]
Tsitologiia. 1986 Aug;28(8):895-6.
3
[Method of purifying and determining glutaraldehyde concentration by electron microscopy and cytochemistry].[通过电子显微镜和细胞化学纯化及测定戊二醛浓度的方法]
Eksp Med Morfol. 1977;16(2):110-4.
4
Detection of impurities in aqueous solution of glutaraldehyde by high performance liquid chromatography with a multichannel photodiode array UV detector.采用带多通道光电二极管阵列紫外检测器的高效液相色谱法检测戊二醛水溶液中的杂质。
J Electron Microsc (Tokyo). 1987;36(3):136-8.
5
Separation of glutaraldehyde and some of its aldol condensation products by hydroxyl-aldehyde group affinity chromatography.
J Biochem Biophys Methods. 1991 May-Jun;22(4):321-9. doi: 10.1016/0165-022x(91)90038-x.
6
The use of glutaraldehyde and tannic acid to preserve reconstituted collagen for electron microscopy.使用戊二醛和鞣酸保存用于电子显微镜检查的重组胶原蛋白。
Histochemistry. 1981;73(1):115-20. doi: 10.1007/BF00493137.
7
The effects of fixation by combination of glutaraldehyde/dimethyl suberimidate. Use of collagen as a model system.戊二醛/辛二亚胺二甲酯联合固定的效果。以胶原蛋白作为模型系统的应用。
J Histochem Cytochem. 1983 Nov;31(11):1274-8. doi: 10.1177/31.11.6194203.
8
Use of high concentrations of glutaraldehyde for immunocytochemistry of transmitter-synthesizing enzymes in the central nervous system.
Neuroscience. 1986 Aug;18(4):975-90. doi: 10.1016/0306-4522(86)90112-0.
9
Glutaraldehyde nonfixation of isolated viral and yeast RNAs.戊二醛对分离出的病毒和酵母核糖核酸的非固定作用
J Histochem Cytochem. 1980 Apr;28(4):311-5. doi: 10.1177/28.4.6768793.
10
Improved utilization of tissue blocks for electron microscopy. Effect of various concentrations of formaldehyde and glutaraldehyde.提高用于电子显微镜检查的组织块的利用率。不同浓度甲醛和戊二醛的作用。
Acta Anat (Basel). 1979;104(4):388-93. doi: 10.1159/000145089.

本文引用的文献

1
Cytochemistry and electron microscopy. The preservation of cellular ultrastructure and enzymatic activity by aldehyde fixation.细胞化学与电子显微镜术。醛类固定对细胞超微结构及酶活性的保存作用。
J Cell Biol. 1963 Apr;17(1):19-58. doi: 10.1083/jcb.17.1.19.
2
Purification and quantitation of glutaraldehyde and its effect on several enzyme activities in skeletal muscle.戊二醛的纯化与定量及其对骨骼肌中几种酶活性的影响。
J Histochem Cytochem. 1967 Aug;15(11):652-61. doi: 10.1177/15.11.652.
3
Glutaraldehyde--its purity and stability.戊二醛——其纯度与稳定性。
Histochemie. 1972;30(2):162-7. doi: 10.1007/BF01444063.
4
The impurities in commercial glutaraldehyde and their effect on the fixation of brain.
J Ultrastruct Res. 1970 Feb;30(3):275-87. doi: 10.1016/s0022-5320(70)80063-6.
5
A comparison of three different electron microscopical grade glutaraldehydes used to fix ovarian tissue.用于固定卵巢组织的三种不同电子显微镜级戊二醛的比较。
J Microsc. 1974 Jul;101(Pt 2):127-41. doi: 10.1111/j.1365-2818.1974.tb03876.x.