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220℃超深井固井水泥浆体系的评价与优化

Evaluation and Optimization of Cement Slurry Systems for Ultra-Deep Well Cementing at 220 °C.

作者信息

Zhang Zhi, Ai Zhengqing, Yang Lvchao, Zhang Yuan, Pang Xueyu, Yuan Zhongtao, Liu Zhongfei, Sun Jinsheng

机构信息

R&D Center for Ultra Deep Complex Reservoir Exploration and Development, CNPC, Korla 841000, China.

Engineering Research Center for Ultra-Deep Complex Reservoir Exploration and Development, Xinjiang Uygur Autonomous Region, Korla 841000, China.

出版信息

Materials (Basel). 2024 Oct 28;17(21):5246. doi: 10.3390/ma17215246.

Abstract

With the depletion of shallow oil and gas resources, wells are being drilled to deeper and deeper depths to find new hydrocarbon reserves. This study presents the selection and optimization process of the cement slurries to be used for the deepest well ever drilled in China, with a planned vertical depth of 11,100 m. The bottomhole circulating and static temperatures of the well were estimated to be 210 °C and 220 °C, respectively, while the bottomhole pressure was estimated to be 130 MPa. Laboratory tests simulating the bottomhole conditions were conducted to evaluate and compare the slurry formulations supplied by four different service providers. Test results indicated that the inappropriate use of a stirred fluid loss testing apparatus could lead to overdesign of the fluid loss properties of the cement slurry, which could, in turn, lead to abnormal gelation of the cement slurry during thickening time tests. The initial formulation given by different service providers could meet most of the design requirements, except for the long-term strength stability. The combined addition of crystalline silica and a reactive aluminum-bearing compound to oil well cement is critical for preventing microstructure coarsening and strength retrogression at 220 °C. Two of the finally optimized cement slurry formulations had thickening times more than 4 h, API fluid loss values less than 50 mL, sedimentation stability better than 0.02 g/cm, and compressive strengths higher than 30 MPa during the curing period from 1 d to 30 d.

摘要

随着浅层油气资源的枯竭,人们不断钻至越来越深的深度以寻找新的油气储量。本研究介绍了用于中国有史以来最深井(计划垂直深度为11100米)的水泥浆的选择和优化过程。该井的井底循环温度和静态温度分别估计为210℃和220℃,而井底压力估计为130MPa。进行了模拟井底条件的实验室测试,以评估和比较四家不同服务提供商提供的水泥浆配方。测试结果表明,不恰当地使用搅拌失水测试仪器可能导致水泥浆失水性能的过度设计,进而导致水泥浆在稠化时间测试期间出现异常胶凝。除了长期强度稳定性外,不同服务提供商给出的初始配方可以满足大多数设计要求。向油井水泥中联合添加结晶二氧化硅和含活性铝的化合物对于防止在220℃下微观结构粗化和强度衰退至关重要。最终优化的两种水泥浆配方在1天至30天的养护期内,稠化时间超过4小时,API失水值小于50毫升,沉降稳定性优于0.02克/立方厘米,抗压强度高于30MPa。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8368/11547183/0fce68fd2119/materials-17-05246-g001.jpg

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