Xie Yun, Jiang Jianqiao, Cui Miao, Chen Yiwen, Li Yongkang, Hu Yue, Yin Ruonan, Ma Xiaomei, Niu Jianming, Cheng Weidong, Gao Feifei
Key Laboratory of Agricultural Product Processing and Quality Control of Specialty (Co-construction by Ministry and Province), School of Food Science and Technology, Shihezi University, Shihezi, Xinjiang 832000, China.
Key Laboratory for Food Nutrition and Safety Control of Xinjiang Production and Construction Corps, School of Food Science and Technology, Shihezi University, Shihezi, Xinjiang 832000, China.
Food Chem X. 2024 Nov 7;24:101978. doi: 10.1016/j.fochx.2024.101978. eCollection 2024 Dec 30.
To investigate the effects of origin and storage time on wine quality, HPLC and HS-SPME-GC-MS were employed to analyze the chemical compositions and VOCs of Cabernet Sauvignon wines from four sub-regions in Xinjiang and with five storage times. Results showed that most of the organic acids were reduced and the anti-oxidant activity decreased during storage. Wines from different regions exhibited differences in the contents of gallic acid, (+)-catechin and (-)-epicatechin. A total of 68 VOCs were identified, with esters and alcohols being the most dominant VOCs. In total, nine VOCs with OAV > 1 were detected in all samples, impacting wine flavor. Cabernet Sauvignon wines were differentiated using PCA and OPLS-DA. 15 and 17 chemical markers were screened based on VIP > 1 for wine of different sub-regions and bottle storage times, respectively. This research provides a data reference for quality characterization of wines obtained from different sub-regions and bottle storage times in Xinjiang.
为研究产地和贮藏时间对葡萄酒品质的影响,采用高效液相色谱法(HPLC)和顶空固相微萃取-气相色谱-质谱联用法(HS-SPME-GC-MS)分析了新疆四个子产区、贮藏时间为五个阶段的赤霞珠葡萄酒的化学成分和挥发性有机化合物(VOCs)。结果表明,贮藏期间大多数有机酸含量降低,抗氧化活性下降。不同产区的葡萄酒在没食子酸、(+)-儿茶素和(-)-表儿茶素含量上存在差异。共鉴定出68种VOCs,其中酯类和醇类是最主要的VOCs。所有样品中共检测到9种气味活性值(OAV)>1的VOCs,影响葡萄酒风味。采用主成分分析(PCA)和正交偏最小二乘法判别分析(OPLS-DA)对赤霞珠葡萄酒进行区分。分别基于变量重要性投影(VIP)>1,为不同子产区和瓶贮时间的葡萄酒筛选出15个和17个化学标志物。本研究为新疆不同子产区和瓶贮时间葡萄酒的品质表征提供了数据参考。