Erni Makita, Hart A John, Trumper David, Owens Crystal E
Department of Mechanical Engineering, Massachusetts Institute of Technology, Cambridge, MA, USA.
Computer Science and Artificial Intelligence Laboratory, Cambridge, MA, USA.
Sci Rep. 2024 Dec 4;14(1):30187. doi: 10.1038/s41598-024-76494-8.
Rheology describes the flow of fluids from food and plastics, to coatings, adhesives, and 3D printing inks, and is commonly denoted by viscosity alone as a simplification. While viscometers adequately probe Newtonian (constant) viscosity, most fluids have complex viscosity, requiring tests over multiple shear rates, and transient measurements. As a result, rheometers are typically large, expensive, and require additional infrastructure (e.g., gas lines), rendering them inaccessible for regular use by many individuals, small organizations, and educators. Here, we introduce a low-cost (under USD$200 bill of materials) Open Source Rheometer (OSR), constructed entirely from thermoplastic 3D printed components and off-the-shelf electromechanical components. A sample fluid rests in a cup while a micro stepping motor rotates a tool inside the cup, applying strain-controlled shear flow. A loadcell measures reaction torque exerted on the cup, and viscosity is calculated. To establish the measurement range, the viscosity of four Newtonian samples of 0.1-10 Pa.s were measured with the OSR and compared to benchmark values from a laboratory rheometer, showing under 23% error. Building on this, flow curves of three complex fluids - a microgel (hand sanitizer), foam (Gillette), and biopolymer solution (1% Xanthan Gum) - were measured with a similar error range. Stress relaxation, a transient test, was demonstrated on the biopolymer solution to extract the nonlinear damping function. We finally include detailed exposition of measurement windows, sources of error, and future design suggestions. The OSR cost is ∼1/25th that of commercially available devices with comparable minimum torque (200 µN.m), and provides a fully open-source platform for further innovation in customized rheometry.
流变学描述了从食品、塑料到涂料、粘合剂以及3D打印墨水等各种流体的流动情况,通常仅用粘度来简单表示。虽然粘度计能够充分测量牛顿(恒定)粘度,但大多数流体具有复杂粘度,需要在多个剪切速率下进行测试以及进行瞬态测量。因此,流变仪通常体积庞大、价格昂贵,并且需要额外的基础设施(如气体管道),这使得许多个人、小型组织和教育工作者无法经常使用。在此,我们介绍一种低成本(材料成本低于200美元)的开源流变仪(OSR),它完全由热塑性3D打印部件和现成的机电部件构建而成。样品流体置于一个杯子中,同时一个微步电机在杯子内部旋转一个工具,施加应变控制的剪切流。一个测力传感器测量施加在杯子上的反作用力矩,并计算粘度。为确定测量范围,使用OSR测量了四种0.1 - 10 Pa·s的牛顿样品的粘度,并与实验室流变仪的基准值进行比较,误差低于23%。在此基础上,测量了三种复杂流体——微凝胶(洗手液)、泡沫(吉列)和生物聚合物溶液(1%黄原胶)——的流动曲线,误差范围相似。对生物聚合物溶液进行了应力松弛这一瞬态测试,以提取非线性阻尼函数。我们最后详细阐述了测量窗口、误差来源以及未来的设计建议。OSR的成本约为具有可比最小扭矩(200 µN·m)的市售设备的1/25,并为定制流变学的进一步创新提供了一个完全开源的平台。